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VOC analysis results, sample AE10240, May 3, 2002

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Laboratory report for volatile organic compounds in sample AE10240 dated May 3, 2002.

NYC-WTC_000082778–000082898

Folder label: “524 5/3/02 - 5/4/02

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Data File C:\MSDchem\l\5973N\02may03\10244.D Vial: 14 Acq On 3 May 2002 8:15 pm Operator: Sample nyc Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: Lscint.p Quant Time: May 03 20:57:01 2002 Quant Results File: W050302.RES Quant Method : C:\MSDCHEM\1...\W050302.M (RTE Integrator) Title : VOC method 8260 Last Update : Fri May 03 14:58:46 2002 Response via : Initial Calibration DataAcq Meth : W050302

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Difluorobenzene 17.71 114 1133128 5.00 ug/L 0.00 27) Chlorobenzene-d5 25.47 117 1047525 5.00 ug/L 0.00 51) 4-Dichlorobenzene-d4 31.54 150 793662 5.00 ug/L 0.00 System "Monitoring Compounds 2) 1,2-Dichloroethane-d4 16.78 65 218000 5.27 ug/L 0.00 Spiked Amount 5.000 Recovery = 105.40% 17) Toluene-d8 21.62 98 1567197 5.03 ug/L 0.00 Spiked Amount 5.000 Recovery = 100.60% 54) 4-Bromofluorobenzene 28.51 95 475284 5.05 ug/L 0.00 Spiked Amount 5.000 Recovery = 101.00% Target Compounds Qvalue

(#) = qualifier out of range (m) =■ manual integration 10244.D W050302.M Fri May 03 20:57:02 2002 Page 1

NYC-WTC_000082827

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NYC-WTC_000082827Source: NYC Law Department, mirrored locally

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