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VOC analysis results, sample AE10240, May 3, 2002

Machine-extracted title · confidence 90%

Laboratory report for volatile organic compounds in sample AE10240 dated May 3, 2002.

NYC-WTC_000082778–000082898

Folder label: “524 5/3/02 - 5/4/02

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Data File C:\MSDCHEM\l\5973N\02MAY03\10240.D Vial: 11 Acq On 3 May 2002 5:55 pm Operator: Sample nyc Inst : Instrumen Mise Multiplr: I.00 MS Integration Params: LSC.P

Quant Method : C:\MSDCHEM\1...\W050302.M (RTE Integrator) Title : VOC method 8260 Library : C:\DATABASE\WILEY7N.L ********************************************************************* Peak Number 3 1-Hexanol, 2-ethyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 30.48 0.46 ug/L 284752 1,4-Dichlorobenzene-d4 31.54 Hit# of 5 Tentative ID MW MolForm CAS# Qual ------------------ 1 1-Hexariol, ■2-ethyl- 130 C8H18O 000104-76-7 90 2 1-Hekanol, 2-ethyl- (CAS) $$ 2-E... 130 C8H18O 000104-76-7 86 3 1-Hexanol, 2-ethyl- (CAS) $$ 2-E... 130 C8H18O 000104-76-7 86 4 2 ETHYL HEXANOL 130 C8H18O 000104-76-7 86 /Kbundance Scan 2699 (30.477 min): 10240.D (-) m/z57.10 100.00% 5)7

41 5000

70 83 T-r 30.20 30.40 30.60 30.80 51, m/z 41710 49.21% 0 •n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #26914; 1-Hexanol, 2-ethyl- 5(7

5000 T-ryr-T 30.20 30.40 30.60 30.80 70 83 43.10 38.96% m/z 0 p" '1,1" (i'"i"" I'l' "I lln|""|il ip-rr ................... ............ nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #26915:1 -Hexanol, 2-ethyl- (CAS) $$ 2-Ethylhexanol $$ 2-E... 5)7 - 30.20 30.40 30.60 30.80 5000 m/z 55.10 32.66%

70 83

0 I'"' I' I" I"" I"'' I' I'' I"" I +rT ..... I... ..... 1...... ....... Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 Abundance #26924:1 -Hexanol, 2-ethyl- (CAS) $$ 2-Ethylhexanol $$ 2-E... 5(7 30.20 30.40 30.60 30.80 m/z 56.10 27.60% 5000 70 83 TTp-nyTTTTp-rTTyrr^^ ......... ................. 112.......... 0 T+yr .... ’ I" " I' 11' I" " I" ‘' I' I "I" " I" -nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110115120 30.20 30.40 30.60 30.80

10240.D W050302.M Mon May 06 12:25:41 2002 Page 5

NYC-WTC_000082807

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NYC-WTC_000082807Source: NYC Law Department, mirrored locally

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