VOC analysis results, sample AE10240, May 3, 2002

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Data File C:\MSDCHEM\l\5973N\02MAY03\0503C10.D Vial: 2 Acq On 3 May 2002 9:20 am Operator: Sample cal 10 Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: Lscint.p Quant Time: May 03 15:07:07 2002 Quant Results File: W050302.RES

Quant Method : C:\MSDCHEM\1...\W050302.M (RTE Integrator) Title : VOC method 8260 Last Update : Fri May 03 14:58:46 2002 . Response via : Initial Calibration DataAcq Meth : W042302

Compound R.T. Qlon Response Cone Unit Qvalue

36) Toluene 21.83 91 2611951 10.55 ug/L 100 37) t-^ans-1,3-Dichloropropene 22.20 75 346244 10.53 ug/L 100 3 8) 2 yHexanone 22.54 43 345505 43.12 ug/L 100 39) 1 ,i ,'2-Trichloroethane 22.63 97 194564 10.19 ug/L 100 40) 1,3-Dichloropropane 23.25 76 357350 10.48 ug/L 100 41) Tetrachloroethene 23.51 166 526855 10.47 ug/L 100 42) Dibromochloromethane 24.02 129 200876 10.56 ug/L 100 43) 1,2-Dibromoethane 24.55 107 160518 10.45 ug/L 100 44) Chlorobenzene 25.58 112 1515330 10.53 ug/L 100 45) 1,1,1;2-Tetrachloroethane 25.64 131 363204 10.53 ug/L 100 46) Ethylbenzene 25.64 91 3257784 10.75 ug/L 100 47) P & M-Xylene 25.84 91 5142455 21.76 ug/L 100 48) o-Xylene 26.96 91 2394476 11.07 ug/L 100 49) Styrene 27.04 104 1709659 10.15 ug/L 100 50) Isopropylbenzene 27.82 105 3141921 10.07 ug/L 100 52) Bromoform 28.00 173 88780 10.63 ug/L 100 53) 1,1,2,2-Tetrachloroethane 28.26 83 196823 10.22 ug/L 100 55) 1,2,3-Trichloropropane 28.63 75 159763 10.27 ug/L 100 56) n-Propylbenzene 28.85 91 4012816 10.78 ug/L 100 57) Bromobenzene 29.08 77 902036 10.59 ug/L 100 58) 1,3,5-Trimethylbenzene 29.23 105 2740214 10.84 ug/L 100 59) 2-Chlorotoluene 29.37 91 2209288 10.63 ug/L 100 60) 4-Chlorotoluene 29.48 91 2183528 10.70 ug/L 100 61) tert-Butylbenzene 30.14 119 2443061 10.98 ug/L 100 62) 1,2,4-Trimethylbenzene 30.26 105 2739363 10.85 ug/L 100 63) sec-Butylbenzene 30.68 105 3857830 10.95 ug/L 100 64) p-Isopropyltoluene 31.01 119 3212622 9.92 ug/L 100 65) 1,3-Dichlorobenzene 31.37 146 1191641 10.57 ug/L 100 66) 1,4-Dichlorobenzene 31.63 146 1142007 10.55 ug/L 100 67) n-Butylbenzene 32.06 91 3068956 9.91 ug/L 100 68) 1,2-Dichlorobenzene 32.61 146 901753 10.67 ug/L 100 69) 1,2-Dibromo-3-chloropropan 34.66 157 28465 10.47 ug/L 100 70) Nitrobenzene , 34.92 77 109786 210.49 ug/L 100 71) 1,2,4-Trichlorobenzene 37.42 180 543654 10.68 ug/L 100 72) Hexachlorobutadiene 37.85 225 419929 10.51 ug/L 100 73) Naphthalene 38.41 128 613858 10.42 ug/L 100 74) 1,2,3-Trichlorobenzene 39.34 180 392227 10.69 ug/L 100

(#) = qualifier out of range (m) = manual integration 0503C10.D W050302.M Fri May 03 15:07:08 2002 Page 2

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