VOC analysis results, sample AE09097, April 24, 2002

NYC 9/11 Public Portal Document J- J_ U4. 4- UJV-.t4.J_k-.il V_kJLllj^kJkXiikl U.

Data File C:\MSDCHEM\l\5973N\02APR24\9392.D Vial: 12 Acq On 24 Apr 2002 9:18 pm Operator: Sample nyc Inst : Instrumen Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\MSDCHEM\1...\W042302. M (RTE Integrator) Title : VOC method 8260 Library- : C:\DATABASE\WILEY7N.L

Peak Number 2 Carbon disulfide Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.25 0.11 ug/L 73073 1,4-Difluorobenzene 17.70 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Carbon disulfide 76 CS2 000075-15-0 74 2 Carbon disulfide (CAS) $$ Carbon... 76 CS2 000075-15-0 9 3 Thiourea (CAS) $$ THU $$ 2-Thiou... 76 CH4N2S 000062-56-6 9 4 Carbon disulfide (CAS) $$ Carbon... 76 CS2 000075-15-0 9 /\bundance Scan 751 (11.250 min): 9392.D (-) m/z 76700 100.00% 7^

5000

, , , . I I I . 1 I . . .T| , , , I I , , , 44 11.00 11.20 11.40 11.60 ................ J....... 64.................... ................................ ............... 207 n/z-> 0 Ur Tn/z 44.00 10.36% 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #2250: Carbon disulfide 7^

5000 11.00 11.20 11.40 11.60 “mTz 78.00 9713% 44 0 3" ^'' " 1' ' 1' " ' 1 I“ " I I ■n/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #2246: Carbon disulfide (CAS) $$ Carbon bisulfide $$ Schwe... 7|6

11,00 11.20 11.40 11.60 5000 m/z77.00 2.59%

44 16 u JuuWJ 0 mfe-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #2260: Thiourea (CAS) $$ THU $$ 2-Thiourea $$ Thiuronium $... 76 11,00 11.20 11,40 11.60 m/z64.00 1.13% 43 5000 60

0 TH-nil'll-..... I *P-'"I I"'' I Tl/Z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 11.00 11.20 11.40 11.60

9392.D W032602.M Fri Apr 26,12:01:10 2002 Page 4

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