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← Document results/DEP Box 64/508 Xtract 10/2/01 Anal 10/27/01
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Pesticide analysis results, sample AD23844, October 2001

Machine-extracted title · confidence 85%

DEP laboratory analysis of pesticides and PCBs in environmental sample AD23844, started October 2 and completed October 27, 2001, with compounds listed and detection limits noted.

NYC-WTC_000081220–000081226

Folder label: “508 Xtract 10/2/01 Anal 10/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\HPCHEM\1\DATA\508F\011027B\2TOXC2.D\ECD1A.CH Vial: 68 Signal #2 : C:\HPCHEM\1\DATA\508F\011027B\2TOXC2.D\ECD2B.CH Acq On : 28 Oct 2001 11:32 pm Operator Nefliu Sample : tox cev Inst 104 Mise : Multiplr 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Oct 29 12:13 2001 Quant Results File: 011029T.RES

Quant Method : C:\HPCHEM\1\METHODS\011029T.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES TOXAPHENE?/28/99 Last Update : Mon Oct 15 11:37:22 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 37.15 34.22 901181 1105392 0.212m 0.194m Spiked Amount 0.100 Recovery = 212.00% 194.00% Target Compounds 1) TOXAPHENE PEAK 1 35.43 35.45 135805 109517 3.147m 3.580m 2) TOXAPHENE PEAK 2 39.53 36.98 504551 341042 3.418m 3.278m 3) TOXAPHENE PEAK 3 41.05 39.00 414402 217663 3.507m 3.348m 4) TOXAPHENE PEAK 4 46.09 40.13 467229 312099 3.523m 3.489m 5) TOXAPHENE PEAK 5 46.67 41.21 531709 196847 3.513m 3.461m

(f)-RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2TOXC2.D 011029T.M Mon Oct 29 12:13:15 2001 Page 1

NYC-WTC_000081225

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NYC-WTC_000081225Source: NYC Law Department, mirrored locally

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