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← Document results/DEP Box 64/508 Xtract 10/2/01 Anal 10/27/01
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Pesticide analysis results, sample AD23844, October 2001

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DEP laboratory analysis of pesticides and PCBs in environmental sample AD23844, started October 2 and completed October 27, 2001, with compounds listed and detection limits noted.

NYC-WTC_000081220–000081226

Folder label: “508 Xtract 10/2/01 Anal 10/27/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Signal #1 : C:\HPCHEM\l\DATA\508F\011027B\2PESTC2.D\ECDlA.CHVial: 74 Signal #2 : C:\HPCHEM\l\DATA\508F\011027B\2PESTC2.D\ECD2B.CH Acq On : 29 Oct 2001 2:26 am Operator: Nefliu Sample : pest cev Inst ; 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Oct 29 11:04 2001 Quant Results File: 011029P.RES

Quant Method : C:\HPCHEM\1\METHODS\011029P.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES 9/6/00 Last Update : Sun Oct 21 15:26:52 2001 Response via : Initial Calibration DataAcq Meth : 508F2.M

Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/L ug/L

System Monitoring Compounds 10) S 2,4-DDD SURROGAT 37.15 34.22 898971 998322 0.203 0.202m Spiked Amount 0.200 Recovery = 101.50% 101.00% Target Compounds 1) PROPACHLOR 16.91 15.84 160651 161200 0.224 (/^/. 0.213 2) g-BHC 23.15 20.86 2349736 2889015 0.315 113'/, 0.290 3) HEPTACHLOR 25.85 22.28 542137 692914 0.106 Iio/, 0.095 4) TiLDRIN 28.46 24.36 1142695 1221620 0.124 0.119 5) HEPTACHLOR EPOXI 32.35 29.54 1948005 2194094 0.256 fo/y 0.242 6) 4,4'-DDE 35.76 32.61 3372572 3602805 0.444m(I)/. 0.415 7) DIELDRIN 36.05 33.29 604308 702682 0.082m <437 0.079 8) ENDRIN 38.13 34.33 857407 890998 0.204 104’/. 0.171m 9) METHOXYCHLOR 49.58 41.45 874667 821054 0.463 0.387

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 2PESTC2.D 011029P.M Mon Oct 29 11:04:33 2001 Page 1

NYC-WTC_000081221

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NYC-WTC_000081221Source: NYC Law Department, mirrored locally

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