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← Document results/DEP Box 64/508 9/27/01 Extraction 10/13-10/15 Analysis
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Chlorinated pesticide analysis results, sample AD23650, Oct 2001

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Laboratory report for chlorinated pesticides in sample AD23650 extracted September 27, 2001, with all results below detection limits.

NYC-WTC_000080695–000080703

Folder label: “508 9/27/01 Extraction 10/13-10/15 Analysis

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NYC 9/11 Public Portal Document Quantitation -Report* “ (QT-Reviewed)- Signal #1 : C:\HPCHEM\l\DATA\508F\011012\23650.D\ECDlA.CH-Vial: -58 Signal #2 : C:\HPCHEM\l\DATA\508F\011012\23650.D\ECD2B.CH Acq On : 14 Oct 2001 5:12 am Operator: Nefliu Sample : sample Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Oct 15 11:56 2001 Quant Results File: 011015T.RES

Quant Method : C:\HPCHEM\1\METHODS\011015T.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES TOXAPHENE7/28/99 Last Update : Mon Oct 15 11:37:22 2001 Response via : Initial Calibration DataAcq Meth : 508F.M Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/1 ug/1

System Monitoring Compounds 6) S 2,4-DDD SURROGAT 37.23 34.49 438789 585343 0.101 0.108 Spiked Amount 0.100 Recoveiry = 101.00% 108.00% Target Compounds 1) TOXAPHENE PEAK 1 35.52 35.79 5230 23786 0.171 0.912 # 2) TOXAPHENE PEAK 2 39.48 37.21 2529 18927 0.042 0.208 # 3) TOXAPHENE PEAK 3 40.92f 39.38 2221 6254 0.027 0.115 # 4) TOXAPHENE PEAK 4 0.00 40.64 0 13735 N.D. 0.314 # 5) TOXAPHENE PEAK 5 0.00 41.51 0 10070 N.D. 0.292 #

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 23650.D 011015T.M Mon Oct 15 11:57:01 2001 Page 1

NYC-Wfc_000080700

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NYC-WTC_000080700Source: NYC Law Department, mirrored locally

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