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Chlorinated pesticide analysis results, sample AD23650, Oct 2001

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Laboratory report for chlorinated pesticides in sample AD23650 extracted September 27, 2001, with all results below detection limits.

NYC-WTC_000080695–000080703

Folder label: “508 9/27/01 Extraction 10/13-10/15 Analysis

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NYC 9/11 Public Portal Document Quantitation Report (QT-Reviewed)' --- Signal-#!—:-C : \HPCHEM\1\DATA\508F\011012\23650tD\ECD1A-;CH Vial: 58 Signal #2 : C:\HPCHEM\l\DATA\508F\011012\23650.D\ECD2B.CH Acq On : 14 Oct 2001 5:12 am Operator: Nefliu Sample : sample Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Quant Time: Oct 15 11:09 2001 Quant Results File: 011012P.RES Quant Method : C:\HPCHEM\1\METHODS\011012P.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES 9/6/00 Last Update : Fri Sep 28 14:35:02 2001 Response via : Initial Calibration DataAcq Meth : 508F.M Volume Inj. Signal #1 Phase Signal #2 Phase: Signal #1 Info Signal #2 Info : Compound RT#1 RT#2 Resp#l Resp#2 ug/L ug/L

System Monitoring Compounds 10) S 2,4-DDD SURROGAT 37.23 34.49 438819 585260 0.096 0.106 Spilced Amount 0.100 Recovery = 96.00% 106.00% Target Compounds 1) .PROPACHLOR 0.00 16.19 0 5042 N.D. d 0.006 2) g-BHC 23.35 21.36 11814 1630 0.001 0.000 # 3) HEPTACHLOR 25.91 22.61 2687 10623 0.000 0.001 # 4) ALDRIN 27.99f 24.87 4658 6852 0.000 0.001 5) HEPTACHLOR EPOXI 32.49 29.79 3341 4344 0.000 0.000 6) 4,4'-DDE 35.65 32.90 1388 4754 0.000 0.000 # 7) DIELDRIN 36.21 33.39 2024 803 0.000 0.000 # 8) ENDRIN 38.26 0.00 813 0 0.000 N.D. d# 9) METHOXYCHLOR 49.89 41.86 1377 476576 0.001 0.229 #

(f)=RT Delta > 1/2 Window (#)=Amounts differ by > 25% (m)=manual int. 23650.D 011012P.M Mon Oct 15 11:09:14 2001 Page 1

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NYC-WTC_000080696Source: NYC Law Department, mirrored locally

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