Pesticide analysis results, sample AD22578, Sep 2001

NYC 9/11 Public Portal Document Area Percent Report Signal #1 : C:\HPCHEM\l\DATA\508F\010926A\0926END.D\ECDlA.CH Vial: 4 Signal #2 : C:\HPCHEM\l\DATA\508F\010926A\0926END.D\ECD2B.CH Acq On : 26 Sep 2001 6:55 pm Operator: Nefliu Sample : endrin decomposition Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e

Method : C:\HPCHEM\1\METHODS\010927P.M .(Chemstation Integrator) Title ; 508 CHLORINATED PESTICIDES 9/6/00

Signal : O926END.D\ECD1A peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total

1 1.247 1,172 1.259 BV 265 7875 0.24% 0.120% 2 1.284 1,259 1.338 W 797 19650 0.59% 0.299% 3 1.352 1,338 1.382 W 281 4171 0.13% 0.063% 4 1.438 1,382 1.717 PB 78 7223 0.22% 0.110% 5 2.375 2.082 2.424 BV 107 10716 0.32% 0.163%

6 2.462 2.424 2.490 PV 667 15855 0.48% 0.241% 7 2.522 2.490 2.556 W 887 27217 0.82% 0.414% 8 2.592 2.556 2.811 VB 599 48388 1.46% 0.737% 9 2.937 2.850 3.137 BV 632 27753 0.84% 0.422% 10 3.176 3.137 3.290 W 115 4536 0.14% 0.069%

11 3.348 3.290 3.367 W 104 2617 0.08% 0.040% 12 3.406 3.367 3.492 W 209 10114 0.31% 0.154% 13 3.516 3.492 3.738 W 94 6827 0.21% 0.104% 14 3.818 3.738 3.911 PV 20 1057 0.03% 0.016% 15 4.166 4.075 4.231 BB 13 767 0.02% 0.012%

16 4.533 4.387 4.598 BB 13 632 0.02% 0.010% 17 5.874 5.517 5.892 BB 12 3943 0.12% 0.060% 18 6.099 5.892 6.166 BB 50 4432 0.13% 0.067% 19 6.279 6.168 6.310 BB 12 913 0.03% 0.014% 20 7.553 7.340 7.599 BB 12 963 0.03% 0.015%

21 7.911 7.615 8.041 BB 17 2975 0.09% 0.045% 22 9.242 8.999 9.313 BB 34 1100 0.03% 0.017% 23 11.033 10.874 11.124 BB 31 1626 0.05% 0.025% 24 11.536 11.259 11.620 BB 15 1511 0.05% 0.023% 25 11.767 11.629 11.826 BB 7 600 0.02% 0.009%

26 12,106 11.826 12.188 BB 9 1191 0.04% 0,018% 27 25,432 25.164 25.603 BB 86 7278 0.22% 0,111% 28 29,470 29.167 29.651 BB 218 15738 0.48% 0,240% 29 31.968 31.285 32.156 BB 892 59312 1.79% 0,903% 30 34.353 33.856 34.474 BB 259 14544 0.44% 0,221%

31 34.569 34.474 34.632 BB 16 814 0.02% 0.012% 32 36.152 35.590 36.277 BB 956 48021 1.45% 0.731% 33 36.489 36.395 36.643 BB 15 1036 0.03% 0.016% 34 38.376 38.212 38.441 BB 16 929 0.03% 0.014% 35 38.658 38.441 39.273 BB 43386 3312549 100.00% 50^J2^ 36 39.469 39.273 39.635 BB 1443 95904 2.90% 1.460% 37 40.007 39.681 40.408 BB 240 20838 0.63% 0.317% 38 40.487 40.410 40.665 BB 14 914 0,03% 0.014% 39 41.627 41.217 42,147 BB 23599 2002899 ^<3746 % 30.491% 40 42.365 42.147 A2-.890 BB 4351 391840 11.83% 5.965%

41 43.372 43.037 43.599 BB 43 6111 0.18% 0.093% 42 44.313 43.995 44.541 BB 187 17689 0.53% 0.269% 43 47.741 47.390 47.878 BB 32 3267 0.10% 0,050% 44 48.282 48.153 48.509 BB 10 932 0.03% 0,014% 45 50.884 50.547 51.172 BB 420 56053 1.69% 0,853%

46 51.503—51.170---- 5-1-. 87-7---- BK 2149 4.396% ■4TT2.I93 51.877 52.498 BB 67 8777 0.26% 0.134%

Sum of corrected areas: 6568893 Signal #2 0926END.D\ECD2B

NYC-WTC_000079103