DDT metabolite analysis results, sample AD22358

NYC 9/11 Public Portal Document Area Percent Report .Signal #1 : C:\HPCHEM\l\DATA\508F\010917\0917END.D\ECDlA.CH Vial: 6 Signal #2 : C:\HPCHEM\l\DATA\508F\010917\0917END.D\ECD2B.CH Acq On : 18 Sep 2001 9:52 am Operator: Nefliu Sample : ENDRIN DECOMPOSITION Inst : 104 Mise : Multiplr: 1.00 IntFile Signal #1: events.e IntFile Signal #2: events2.e Method : C:\HPCHEM\1\METHODS\010918P.M (Chemstation Integrator) Title : 508 CHLORINATED PESTICIDES 9/6/00 Signal : O917END.D\ECD1A peak R.T. Start End PK peak peak peak % of # min min min TY height area % max. total 1 1.317 1.283 1.372 BV 456 11292 0.76% 0.388% 2 1.386 1.372 1.425 W 251 3757 0.25% 0.129% 3 1.472 1.425 1.692 PB 37 3206 0.22% 0.110% 4 2.396 2.344 2.456 BV 28 882 0.06% 0.030% 5 2.499 2.456 2.528 PV 651 15317 1.03% 0.527% 6 2.561 2.528 2.594 W 825 25506 1.72% 0.877% 7 2.627 2.594 2.847 VB 555 44993 3.04% 1.547% 8 2.977 2.903 3.187 BV 677 28442 1.92% 0.978% 9 3.220 3.187 3.337 VB 84 3275 0.22% 0.113% 10 3.392 3.343 3.412 BV 46 1035 0.07% 0.036% 11 3.450 3.412 3.526 W 98 3783 0.26% 0.130% 12 3.562 3.526 3.621 VB 29 931 0.06% 0.032% 13 5.534 5.116 5.561 BB 5 564 0.04% 0.019% 14 5.919 5.564 5.976 BB 32 1035 0.07% 0.036% 15 6.189 5.993 6.237 BB 40 1865 0.13% 0.064% 16 7.086 6.986 7.159 BB 19 652 0.04% 0.022% 17 8.091 7.370 8.180 BB 51 551 0.04% 0.019% 18 10.987 10.552 10.997 BB 2 679 0.05% 0.023% 19 25.631 25.326 25.746 BB 16 1336 0.09% 0.046% 20 34.495 32.239 34.592 BB 76 4253 0.29% 0.146% 21 35.712 34.591 35.727 BB 8 14414 0.97% 0.495% 22 36.288 35.727 36.400 BB 136 12119 0.82% 0.417% 23 36.686 36.528 36.723 BB 7 512 0.03% 0.018% 24 38.82a 38.588 39.409 BB 20169 1480899 100.00% 50.907% 39~47K-'''3?77B7~- BB —rrv 11889 0.80% 0.409* 26 40.191 40.038 40.371 BB 81 6157 0.42% 0.212% 27 40.690 40.589 40.823 BB 14 1043 0.07% 0.036% 28 41.830 41.558 42.357 BB 11500 974935 65.83% 33.514% 29^2_Sa4. BB 1155 102584 6.93% 3.526% 317 43.237 42.933 43.296 BB S sT? 0.04% 0.018% 31 43.601 43.442 43.938 BB 39 3917 0.26% 0.135% 32 48.452 48.416 48.789 BB 5 669 0.05% 0.023% 33 49.435 49.289 49.656 BB 11 1196 0.08% 0.041% 34 49.988 49.845 50.135 BB 10 975 0.07% 0.034% 35 51.237 50.920 51.519 BB 204 27540 1.86% 0.947% 36 51.868 51.521 ,961 RR 868 116294 7.85% 3.998% Sum of corrected areas: 2909022 Signal #2 0917END.D\ECD2B

1 1.536 1.495 1.556 BV 360 9690 0.49% 0.237% 2 1.573 1.556 1.655 W 798 23902 1.21% 0.584% 3 2.593 1.851 2.703 BV 251 70041 3.55% 1.710% 4 3.201 2.703 3.296 PV 648 209918 10.64% 5.126% 5 3.375 3.296 3.414 W 418 30403 1.54% 0.742% 6 3.546 3.414 3.710 VB 245 34018 1.72% 0.831% 7 3.866 3.819 3.908 W 55 2616 0.13% 0.064% 8 3.931 3.908 4.030 VB 79 4951 0.25% 0.121% 9 4.283 4.039 4.301 BB 12 7188 0.36% 0.176% 10 5.719 5.313 5.731 BB 5 954 0.05% 0.023%

NYC-WTC_000078529