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Chain of custody record, Westchester County Department of Labs

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Custody form for samples handled by the Westchester County Department of Labs & Research.

NYC-WTC_000072138–000072145

Folder label: “26624

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NYC 9/11 Public Portal Document

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13.1.1 3 SOP'S - ICR manifold, well-slide. Method 1623 13.1.2 1 QAP - describing all laboratory calibrations and quality control practices 13.1.3 1 QAPP - Routine Keypoint Protozoan Monitoring

13.2 QC Per sample 13.2.1 Postive and negative control slides are prepared with each sample to ensure stain performance, and comparative cyst and oocyst appearance. Results are pass/fail.

13.3 Weekly or Biweekly QC (equivalent to “Batch" QC) 13.3.1 Positive and negative spikes are added to carboys of DI water, filtered and taken through the entire ICR analytical procedure to ensure the negative spike remains negative and the positive spike results in recovery. Results are recorded as percent recovery. 13.3.2 Positive and negative spikes are added to carboys of DI water, filtered and taken through the entire Method 1623 analytical procedure to ensure the negative spike remains negative and the positive spike results in recovery. Results are recorded as percent recovery.

13.4 Monthly or Bimonthly QC 13.4.1 Precision of microscopic counts is performed between principle analysts for both cysts and oocysts by replicate counting of the same slides of unknown concentration.

13.5 Quarterly QC 13.5.1 The DEP is registered to electively participate in the EPA PE program for the ICR manifold method and for Method 1623. Samples are delivered quarterly for ongoing precision and recovery.

13.6 Method Specific QA/QC 13.6.1 Since all methods have different specific QA/QC this information can be found in the respective SOP's.

14 Data Reduction, Verification, Validation, and Reporting

14.1 Calculations are deteimined according to the formula used in the April 1996 ICR on pageVII-28 to VII-30. 14.2 No calculations are necessaiy for samples processed using the 1623 method. Direct counts ai'e recorded. 14.3 Before data is reported it is checked by the principal analyst and compared to the laboratoiy notebook. 14.4 The results ai'e validated by coixectly processing the QC samples and the weekly batch samples and as well as passing internal Q.C. inspection by lab director and Q.C. inspector.

QUAL1080D02.doc Page 10 of 11

NYC-WTC_000072143

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NYC-WTC_000072143Source: NYC Law Department, mirrored locally

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NYC-WTC_000070918 · Box DEP Box 61

Chain of custody form for samples submitted to the Westchester County Department of Labs and Research in Valhalla, NY.

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