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Water analysis report, NYC DEP, GCMS field blank, Nov-Dec 2001

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Laboratory analysis of a field blank water sample collected November 20, 2001, testing for unknown compounds via GCMS.

NYC-WTC_000071054–000071058

Folder label: “28427

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NYC 9/11 Public Portal Document

REPORT OF ANALYSIS Westchester County Department of Labs and Research 2 Dana Road Valhalla, New York

Agency: New York City DEP DWQC Sample FIELD BLANK Distribution Laboratory 96-05 Horace Harding Ex. Corona N.Y. 11368 Sample FBD Dr. Ian Hurley ID of Source: Received KM Collection 11/20/2001 AT Bottle p1109,q943 Submitted 11/20/2001 AT Collected By: LAB Sample Type: POT_DW Comment: PWS No.: Source Code: Type Descriptor: Sample chilled on arrival? : YES Report

Sample No. AD28427 Method Test Description Results Units MDL Analyzed on Validator Organics GCMS Scan For Unknowns Other unknown compounds ug/L 11/21/2001 DLV The GCMS scan, from 35 to 550 amu, does not reveal the presence of unusual compounds. However, di-n-butylphthalate is present at an estimated level of 0.28 ug/L. The recovery for the Surrogate Standard in this sample was 68%. Recoveries for 41 of the 44 compounds in the LSC Standard were outside of EPA 625 acceptance ranges, soon however, GCMS method acceptance ranges will be established and used instead.

Approved Pam Dilsizian QA Officer Date Approved: 1/31 /2002

Environmental Laboratories emailed Original 1/31/2002

NYS ELAP# 10108 Page 1 of 1

NYC-WTC_000071054

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NYC-WTC_000071054Source: NYC Law Department, mirrored locally

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Field blank analysis report, GCMS, Nov 2001 · Box DEP Box 61

NYC-WTC_000070792

Laboratory field blank analysis report for NYC DEP water samples collected on November 22, 2001, using gas chromatography mass spectrometry.

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Form documenting the chain of custody for samples submitted to the Westchester County Department of Labs and Research.

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