GC/MS analysis report for sample AD25839, Dec 2001

NYC 9/11 Public Portal Document

Quantitatic n QT Reviewci) Data File : C:\IIPCHEM\1\DATA\NOV1901 3.1 Vial: 4 Acq On : 19 Nov 2001 6:12 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Dec 5 15:01 2001 C -t Jesuits File: NP103001.RES Quant Method : C: \HPCHEM\l\METHODS\i:r If 01 RT Integrator) Title : 209 625/TCLP calibrate cn th Last Updace : Fri Nov 02 16:41:16 2C02 Response via : Initial Calibration DataAcq Meth : NP103001

Internal Standards R.T. I ■ "onre Cone Units Dev(Min) 1) 1,4-Dichlorobenzene-d4 11.71 2 34: 20.00 ug/1 -0.01 19) Naphthalene-d8 15.32 ' 31' 20.00 ug/1 -0.01 31) Acenaphthene-dlO 20.60 lo; 20.00 ug/1 -0.01 49) Phenanthrene-dlO 25.02 55 a 20.00 ug/1 -0.01 59) Chrysene-dl2 33.0.- 27. 20.00 ug/1 -0.01 68) Perylene-dl2 37. If 80i 20.00 ug/1 0.00 System Monitoring Compounds 4) 2-Fluorophenol 0.00 C 0.00 ug/1 Spiked Amount 7E.000 ’ecf very = 0.00% 5) Phenol-d5 0.00 ) ( O.OC' ug/1 Spiked Amount 75.000 eci very = 0.00% 6) 2 -Chlorophenol-d4 11.70 76' 0. C1 ug/1 0.47 Spiked Amount 75.000 ec very = 0.01% 7) 1,2-Dichlorobenzene-d4 12.2: 15 0.07 ug/1 -0.04 Spiked Amount 50.000 ec "ery - 0.06% 20) Nitrobenzene-d5 0.0 O.C ug/1 Spiked Amount 50.000 ec very = 0.00% 32) 2-Flucrobiphenyl 18.74 .19'. 0.02 ug/1 0.13 Spiked Auiount 5C .000 ecc very = 0.04% 33) 2,4,6-Tribromophenol 0.00 ( 0.0^' ug/1 Spiked Amount 75.000 'ecc very = 0.00% 62) Terphenyl-dl4 0.0^ t 0 . ( ug/ i Spiked Amount 50.000 ec very - 0.00% Targer Compounds Qvalue 2) Pyridine 0.0' Nk . 3) N-nitroso-dimethyl amine O.Ot N. 2. 8) Phenol 0.0 N . 9) bis(2-Chloroethyl)ether O.Oi N.I. 10) 2-Chlorophenol 0.0' N.: . 11) L,3-Da chlorobenzene 0.0( ( N. D. 12) 1,4-Dichlorobenzene 0.0^ ( N.D. 13) 1,2-Dichlorobenzene 0.0- f N. D. 14) 2-Methylphenol 0.0' N. 15) 2,2'-oxybis(1-Chloropropan O.OC N.I. 16) 3&4-Methylphenol o.oc N. 2.. 17) N-Mitroso-di-n-propylamine O.OC ) N. 2. 18) Hexachloroethane 0.0' N. ■:. 21) .Nitrobenzene o.c 22) Isophorone 0.0 r.. . (#) = qualifier out of range (m) = ma . nte ti n 25830.D NP103001.M Wed Dec 05 • <6 2 Page 1

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