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GCMS analysis results, sample AD25463, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25463 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069687–000069696

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C;\HPCHEM\1\DATA\NOV1601\25463.D Vial; 6 Acq On : 16 Nov 2001 7:55 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing ; OFF Filtering: 5 Sampling ; 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation; 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 7.689 284 288 312 rBV 109047 359987 6.90% 1.297% 2 11.710 721 726 748 rBV 1355985 3602167 69.07% 12.982% 3 15.318 1113 1119 1136 rBV 2183304 4753643 91.15% 17.131% 4 20.597 1687 1694 1719 rBV 2396468 5215046 100.00% 18.794% 5 25.022 2169 2176 2188 rBV2 2255602 5075040 97.32% 18.289%

6 25.159 2188 2191 2203 rVB2 16158 52993 1.02% 0.191% 7 33.054 3044 3051 3066 rBV2 2009490 4597740 88.16% 16.569% 8 37.158 3487 3498 3520 rBV 1431971 4091794 78.46% 14.746%

Sum of corrected areas: 27748410 25463.D NP103001.M Wed Nov 21 11:58:35 2001

NYC-WTC_000069693

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NYC-WTC_000069693Source: NYC Law Department, mirrored locally

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