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GCMS analysis results, sample AD25461, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25461 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069659–000069675

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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NYC 9/11 Public Portal Document

Library Search-Compound Report Data File : C:\HPCHEM\1\DATA\NOV1601\25461.D Vial: 3 Acq On ; 16 Nov 2001 4:59 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 3-Isopropoxy-l,1,1,7,7,7-hexam Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 47.13 0.52 ug/1 102124 Perylene-dl2 37.15 Hit# of 5 fentative ID MW MolForm CAS# Qual 1 3-Isoproppky-l,1,1,7,7,7-hexamethyl 576 C18H52O7Si7 071579-69-6 25 2 Tris (trWethylsilyl)borate 278 C9H27BO3Si3 004325-85-3 22

uu 3 Trisil :ane, octamethyl- 236 C8H24O2Si3 000107-51-7 22 4 2,6-D^ iethyl-3,4-bis(trimethylsilyl 311 C15H29NO2Si2 000000-00-0 16 Abundance / Scan 4584 (47.130 min): 25461.D (-) "m/z 72795 100.00% 7b 147 221

5000 281 355 44 429 46.80 47.00 47.20 47.40

■n/z-> JU 100 150 200 250 300 350 400 450 500 550 50 I ii m/z 147.00 80.84% Abundance #60503: 3-lsopropoxy-1,1,1,7,7,7-hexamethyl-3,5,5-tris(trim 73

5000 147 m/z 221.05 75.87%

•n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #39028: Tris(trimethylsilyl)borate 7b 221 ... ^.80 47.00 47.20 47.40 5000 m/z 281.00 32.46% 263 133 175

•n/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance #71066: Trisiloxane, octamethyl- 73 211 <^.80 47.00 47.20 47.40 m/z 207.00 29.14% 5000

103 133 189 I I .I .I T-^T^U-rTn-rn-ry-r-T-r-T-rr-rn-T-r-r-rn-ry-^^

■n/z~> 50 100 150 200 250 300 350 400 450 500 550 46.80 47.00 47.20 47.40

25461.D NP103001.M Wed Nov 21 11:43:34 2001 Page 7

NYC-WTC_000069674

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NYC-WTC_000069674Source: NYC Law Department, mirrored locally

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