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GCMS analysis results for sample AD25156, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD25156 conducted on November 28, 2001, noting unknown compounds.

NYC-WTC_000069509–000069518

Folder label: “GCMS Scan X 10/24/01 An 11/9/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0901\25045.D Vial: 19 Acq On : 10 Nov 2001 5:57 am Operator: 209 GALOS Sample : gc/ras unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Librairy : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.32 ug/1 219581 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 ihtative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 78 2 tert-Butyl Hydroperoxide 90 C4H10O2 000075-91-2 25 3 2-Prop^ol, 2-methy 1- 74 C4H1O0 000075-65-0 17 4 Acetone 58 C3H6O 000067-64-1 12 Abundance / Scan 289 (7.695 min): 25045.D (-) m/z 42.95 100.00% 43

59 5000

101 7.^ 7.60 7.80 8.00

nfe-> (iiii'|Wii|ri'l' T ^4...,...,.. 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 207 m/z 59.05 50.91% Abundance #64274:2-Pentanone. 4-hydroxy-4-methyl- 4(3

5000 Z4O7^ 7.80 59 8.00 m/z 101.05 21.28% «« 10'’ ’P‘” 1‘ jTTTTp-rrrj- mfe-> 20 30 40 50 60 70 80 90 10011012012)14015016017018012)200210 fiibundance #922: tert-Butyl Hydroperoxide

43 ' ’7.46 7.60 7.80 8.00 5000 m/z 58.05 18.23%

31 , I 11 ■ 1111 1111 >. 1111 > 111 ’ I' * *' I ‘ m/z-> 2)30 40 50 60 70 80 90 100110120130140150160170180190200210 Sundance #62572:2-Propanol, 2-mothyl- I.. I . I 53 7.^ 7.60 7.80 8.00 m/z 41.05 6.41% 5000 41

1 I ‘1 ‘ 'I mfe-> 20 30 40 50 60 70 80 90 100110120130140150160170180190 200 210 '7.^' 7.60 7.^ 's.OO

25045.D NP103001.M Wed Nov 28 12:11:56 2001 Page 1

NYC-WTC_000069517

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NYC-WTC_000069517Source: NYC Law Department, mirrored locally

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