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GCMS analysis results for sample AD24333, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24333 with detection of unknown compounds on November 27, 2001.

NYC-WTC_000068737–000068747

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0101\24333.D Vial: 9 Acq On : 1 Nov 2001 10:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.700 285 289 299 rBV 39660 106942 2.61% 0.500% 2 11.574 706 711 721 rBV2 30036 76012 1.86% 0.355% 3 11.712 721 726 750 rVB 1157316 2894972 70.72% 13.528% 4 15.320 1113 1119 1137 rBV 1883616 3958295 96.70% 18.497% 5 20.599 1687 1694 1711 rBV 1899860 4093361 100.00% 19.128% 6 25.014 2169 2175 2188 rBV2 1748071 3916631 95.68% 18.302% 7 33.056 3044 3051 3069 rBV2 1517788 3464249 84.63% 16.188% 8 37.160 3489 3498 3511 rBV2 1011345 2889300 70.59% 13.502%

Sum of corrected areas: 21399762 24333.D NP103001.M Tue Nov 27 08:07:44 2001

NYC-WTC_000068743

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NYC-WTC_000068743Source: NYC Law Department, mirrored locally

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