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GCMS analysis results for sample AD24477, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24477 conducted on November 14, 2001, identifying unknown compounds.

NYC-WTC_000068496–000068506

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\NOV0201\24477.D Vial: 13 Acq On : 3 Nov 2001 2:43 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 7.696 285 289 306 rBV 96627 256599 5.60% 1.062% 2 11.570 707 711 721 rBV 34451 82442 1.80% 0.341% 3 11.708 721 726 743 rBV 1342757 3220704 70.26% 13.332% 4 15.316 1113 1119 1137 rBV 2062227 4403366 96.06% 18.228% 5 20.594 1687 1694 1708 rBV 2152971 4584172 100.00% 18.976% 6 25.019 2169 2176 2187 rBV2 2072832 4403209 96.05% 18.227% 7 33.061 3044 3052 3070 rBV2 1630473 3912365 85.35% 16.195% 8 37.156 3490 3498 3512 rBV2 1180096 3294931 71.88% 13.639%

Sum of corrected areas: 24157788 24477.D NP103001.M Tue Nov 13 10:10:09 2001

NYC-WTC_000068502

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NYC-WTC_000068502Source: NYC Law Department, mirrored locally

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