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GCMS analysis results for sample AD24217, Nov 6 2001

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Laboratory report documenting GCMS analysis of sample AD24217 conducted on November 6, 2001, noting unknown compounds.

NYC-WTC_000068003–000068021

Folder label: “GCMS Scan X 10/10/01 An 11/1/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data Pile : C:\HPCHEM\1\DATA\NOV0101\24216 .D Vial: 3 Acq On : 1 NOV 2001 4:58 pm Operator: 209 GALOS Sanple : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Nov 6 11:28 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NP101901

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 0.00 128 0 N.D. 2 9) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 3 8) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 40) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 20.87 165 490 N.D. 4 5) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 25.02 178 669 N.D. 56) Jtnthracene 25.02 178 669 N.D. 57) Di-n-butylphthalate 27.02 149 7515 N.D. 58) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 0.00 184 0 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 31.54 149 1742 N.D. 65) Benzo(a)anthracene 33.06 228 5308 N.D. 66) Bis(2-ethylhexyl)phthalate 33.33 149 26459 0.27 ug/1 96 67) Chrysene 33.13 228 4151 N.D. 69) Di-n-Octylphthalate 35.07 149 35251 N.D. 70) Benzo(b)fluoranthene 36.08 252 25143 0.31 ug/1 95 (#) = qualifier out of range (m) = manual integration 24216.D NP103001.M Tue Nov 06 11:30:00 2001 Page 2

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NYC-WTC_000068005Source: NYC Law Department, mirrored locally

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