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GCMS analysis results for sample AD24049, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD24049 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067855–000067866

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT2501\24049.D Vial: 10 Acq On : 25 Oct 2001 9:29 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 26 9:51 2001 Quant Results File: NP101901.RES Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Tue Oct 23 10:12:13 2001 Response via : Initial Calibration DataAcq Meth : NPl01901

Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 11.73 152 752572 20.00 ug/1 -0.02 19) Naphthalene-d8 15.34 136 3080943 20.00 ug/1 -0.02 31) Acenaphthene-dlO 20.63 164 1493404 20.00 ug/1 0.00 49) Phenanthrene-dlO 25.06 188 2243004 20.00 ug/1 0.00 59) Chrysene-dl2 33.10 240 1195243 20.00 ug/1 0.00 68) Pei:ylene-dl2 37.21 264 769169 20.00 ug/1 0.01 System Monitoring Compounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 11.72 132 517 0.01 ug/1 0.46 Spiked Amount 75.000 Recovery = 0.01% 7) 1,2-Dichlorobenzene-d4 12.26 152 8778 0.17 ug/1 -0.01 Spiked Amount 50.000 Recovery = 0.34% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.78 172 3367 0.02 ug/1 0.12 Spiked Amount 50.000 Recovery = 0.04% ’ 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery ss 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 24049.D NP101901.M Fri Oct 26 09:52:57 2001 Page 1

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