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GCMS analysis results, sample AD23948, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23948 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067675–000067689

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\HPCHEM\1\DATA\OCT1701\23947.D Vial: 14 Acg On : 18 Oct 2001 2:00 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % Of # min scan scan scan TY height area % max. total

1 5.140 8 11 19 rVB 12290 27608 1.06% 0.200% 2 6.379 142 146 151 rBV 24020 47129 1.80% 0.342% 3 6.480 153 157 167 rW 38283 98368 3.76% 0.713% 4 6.618 169 172 181 rW 19931 44386 1.70% 0.322% 5 6.728 181 184 193 rVB2 27635 57200 2.19% 0.415%

6 7.747 292 295 312 rBV 60798 153416 5.87% 1.112% 7 11.621 711 717 727 rBV 21356 50815 1.94% 0.368% 8 11.759 727 732 745 rBV 753334 1905272 72.89% 13.807% 9 15.376 1120 1126 1144 rBV 1187605 2581594 98.77% 18.709% 10 20.654 1695 1701 1721 rBV 1214558 2613730 100.00% 18.942%

11 25.079 2177 2183 2195 rBV2 1104499 2424755 92.77% 17.572% 12 33.121 3052 3059 3075 rBV2 900568 2079836 79.57% 15.073% 13 37.234 3498 3507 3524 rBV2 614601 1714750 65.61% 12.427%

Sum of corrected areas: 13798859

23947.D NP101901.M Wed Oct 24 11:20:27 2001

NYC-WTC_000067681

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NYC-WTC_000067681Source: NYC Law Department, mirrored locally

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