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GCMS analysis results, sample AD23947, Oct 2001

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DEP lab report for GCMS analysis of sample AD23947 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067651–000067674

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT2301\23915.D Vial: 19 Acq On : 24 Oct 2001 5:24 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 25 12:03 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 14.71 107 176 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 2 8) Naphthalene 15.41 128 119 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 17.27 107 294 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 3 8) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 4 0) Acenaphthylene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 21.08 65 319 N.D. 44) 2,4-Dinitrotoluene 21.24 165 176 N.D. 45) Diethylphthalate 22.13 149 1915 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 22.76 77 271 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 53) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 25.13 178 422 N.D. 56) Anthracene 25.13 178 422 N.D. 57) Di-n-butylphthalate 27.05 149 6736 N.D. 5 8) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 33.08 252 1136 N.D. 61) Benzidine 28.77 184 1369 N.D. 63) Pyrene 29.41 202 359 N.D. 64) Butylbenzylphthalate 31.56 149 1012 N.D. 65) Benzo(a)anthracene 33.10 228 5396 N.D. 66) Bis(2-ethylhexyl)phthalate 33.36 149 13642 N.D. 67) Chrysene 33.10 228 5396 N.D. 69) Di-n-Octylphthalate 35.10 149 3895 N.D. 70) Benzo(b)fluoranthene 36.12 252 1894 N.D. (#) = qualifier out of range (m) = manual integration 23915.D NP101901.M Thu Oct 25 12:03:31 2001 Page 2

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