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GCMS analysis results, sample AD23910, Oct 2001

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Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

NYC-WTC_000067579–000067600

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : Cs\HPCHEM\1\DATA\OCT1801\23910 .D Vial: 5 Acq On : 18 Oct 2001 8:06 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.376 141 145 151 rBV 21502 43504 1.76% 0.328% 2 6.477 151 156 168 rW 33630 90981 3.68% 0.686% 3 6.614 168 171 180 rW 16969 35836 1.45% 0.270% 4 6.724 180 183 190 rW 22369 46277 1.87% 0.349% 5 7.211 230 236 241 rBV2 8881 25319 1.02% 0.191%

6 7.753 292 295 310 rBV 46352 123101 4.98% 0.929% 7 11.627 711 717 727 rBV 19994 47791 1.93% 0.361% 8 11.764 727 732 747 rW 724135 1813310 73.30% 13.681% 9 15.372 1119 1125 1139 rBV 1101459 2438040 98.55% 18.395% 10 20.660 1694 1701 1715 rBV 1137633 2473934 100.00% 18.665%

11 25.085 2176 2183 2195 rBV2 1062216 2320704 93.81% 17.509% 12 33.118 3051 3058 3073 rBV2 884991 2085975 84.32% 15.738% 13 37.231 3497 3506 3527 rBV2 620317 1709356 69.09% 12.897%

Sum of corrected areas: 13254128 23910.D NP101901.M Tue Oct 23 14:33:33 2001

NYC-WTC_000067593

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NYC-WTC_000067593Source: NYC Law Department, mirrored locally

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