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GCMS analysis results, sample AD23904, Oct 2001

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DEP lab report for GCMS analysis of sample AD23904 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067508–000067521

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1701\23904.D Vial: 9 Acq On : 17 Oct 2001 9:08 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 17 21:57 2001 Quant Results File: NP091101.RES Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NPO91101

Compound R.T. Qlon Response Cone Unit Qvalue 23) 2-Nitrophenol 0.00 139 0 N.D. 24) 2,4-Dimethylphenol 0.00 107 0 N.D. 25) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 26) 2,4-Dichlorophenol 0.00 162 0 N.D. 27) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 28) Naphthalene 0.00 128 0 N.D. 29) Hexachlorobutadiene 0.00 225 0 N.D. 30) 4-Chloro-3-methylphenol 0.00 107 0 N.D. 34) Hexachlorocyclopentadiene 0.00 237 0 N.D. 35) 2,4,6-Trichlorophenol 0.00 196 0 N.D. 36) 2,4,5-Trichlorophenol 0.00 196 0 N.D. 37) 2-Chloronaphthalene 0.00 162 0 N.D. 3 8) Dimethylphthalate 0.00 163 0 N.D. 39) 2,6-Dinitrotoluene 0.00 165 0 N.D. 4 0) Acenaphthy1ene 0.00 152 0 N.D. 41) Acenaphthene 0.00 153 0 N.D. 42) 2,4-Dinitrophenol 0.00 184 0 N.D. 43) 4-Nitrophenol 0.00 65 0 N.D. 44) 2,4-Dinitrotoluene 0.00 165 0 N.D. 45) Diethylphthalate 0.00 149 0 N.D. 46) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 47) Fluorene 0.00 166 0 N.D. 48) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 50) 4,6-Dinitro-2-methylphenol 0.00 198 0 N.D. 51) N-Nitrosodiphenylamine 0.00 168 0 N.D. 52) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 5 3) Hexachlorobenzene 0.00 284 0 N.D. 54) Pentachlorophenol 0.00 266 0 N.D. 5 5) Phenanthrene 0.00 178 0 N.D. 56) Anthracene 25.09 178 182 N.D. 57) Di-n-butylphthalate 27.08 149 1584 N.D. 58) Fluoranthene 0.00 202 0 N.D. 60) 3,3'-Dichlorobenzidine 0.00 252 0 N.D. 61) Benzidine 0.00 184 0 N.D. 63) Pyrene 0.00 202 0 N.D. 64) Butylbenzylphthalate 0.00 149 0 N.D. 65) Benzo(a)anthracene 33.12 228 1936 N.D. 66) Bis (2-ethylhiexyl)phthalate 33.39 149 819 N.D. 67) Chrysene 33.12 228 1936 N.D. 69) Di-n-Octylphthalate 0.00 149 0 N.D. 70) Benzo(b)fluoranthene 0.00 252 0 N.D. (#) = qualifier out of range (m) = manual integration 23904.D NP101901.M Tue Oct 23 12:42:35 2001 Page 2

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