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GCMS analysis report, sample AD22558, October 2001

Machine-extracted title · confidence 75%

Gas chromatography-mass spectrometry analysis of sample AD22558 started October 1, 2001, identifying other unknown compounds.

NYC-WTC_000067406–000067424

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

LSC Area Percent Report Data File : C:\HPCHEM\1\DATA\OCT1701\22558.D Vial: 3 Acq On : 17 Oct 2001 3:08 pm Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5 Signal : TIC peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total 1 6.374 142 145 151 rBV 26206 50536 1.89% 0.356% 2 6.484 153 157 167 rVV2 44000 110764 4.15% 0.780% 3 6.613 168 171 176 rW 22052 43980 1.65% 0.310% 4 6.732 180 184 191 rVB 28370 63786 2.39% 0.449% 5 7.742 291 294 301 rBV 91867 205949 7.72% 1.450% 6 (1?>212 559 563 575 rVB 12834 27385 1.03% 0.193% 7 \U)Z423 582 586 593 rBV3 11285 27985 1.05% 0.197% 8 11.625 713 717 727 rBV 21926 49440 1.85% 0.348% 9 11.763 727 732 752 rVB 804116 1907660 71.48% 13.430% 10 15.371 1119 1125 1143 rBV 1121765 2608753 97.75% 18.365% 11 20.659 1694 1701 1714 rBV 1221342 2668875 100.00% 18.788% 12 25.084 2176 2183 2194 rBV2 1178261 2485992 93.15% 17.501% 13 33.126 3051 3059 3074 rBV 931263 2153342 80.68% 15.159% 14 37.238 3499 3507 3522 rBV2 641646 1800463 67.46% 12.675%

Sum of corrected areas: 14204910 22558.D NP101901.M Tue Oct 23 15:08:07 2001

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NYC-WTC_000067412Source: NYC Law Department, mirrored locally

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