NYC-WTC_000067453
DEP lab report for GCMS analysis of sample AD23900 conducted on October 23, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.998
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GCMS analysis report, sample AD22558, October 2001
Machine-extracted title · confidence 75%Gas chromatography-mass spectrometry analysis of sample AD22558 started October 1, 2001, identifying other unknown compounds.
NYC-WTC_000067406–000067424Folder label: “GCMS Scan X 10/2/01 An 10/17/01”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed) Data File : C:\HPCHEM\1\DATA\OCT1701\22558.D . Vial: 3 Acq On : 17 Oct 2001 3:08 pm yJHyiFO Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: RTEINT.P Quant Time: Oct 23 14:54 2001 / Quant Results File: NP091101.RES
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Last Update : Fri Oct 12 09:04:47 2001 Response via : Initial Calibration DataAcq Meth : NP091101
Internal Standards R.T. Qlon Response Cone Units Dev(Min) 1) l,4-Dichlorobenzene-d4 11.76 152 363184 20.00 ug/1 -0.14 19) Naphthalene-d8 15.37 136 1423239 20.00 ug/1 -0.15 31) Acenaphthene-dlO 20.66 164 675067 20.00 ug/1 -0.15 49) Phenanthrene-dlO 25.08 188 968236 20.00 ug/1 -0.15 59) Chrysene-dl2 33.13 240 698594 20.00 ug/1 -0.15 68) Perylene-dl2 37.24 264 501905 20.00 ug/1 -0.18 System Monitoring Confounds 4) 2-Fluorophenol 0.00 112 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 5) Phenol-d5 0.00 99 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 6) 2-Chlorophenol-d4 0.00 132 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 7) 1,2-Dichlorobenzene-d4 12.29 152 3667 0.21 ug/1 -0.14 Spiked Amount 50.000 Recovery = 0.42% 20) Nitrobenzene-d5 0.00 82 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% 32) 2-Fluorobiphenyl 18.80 172 1302 0.03 ug/1 0.00 Spiked Amount 50.000 Recovery s 0.06% 33) 2,4,6-Tribromophenol 0.00 330 0 0.00 ug/1 Spiked Amount 75.000 Recovery = 0.00% 62) Terphenyl-dl4 0.00 244 0 0.00 ug/1 Spiked Amount 50.000 Recovery = 0.00% Target Compounds Qvalue 2) Pyridine 0.00 79 0 N.D. 3) N-nitroso-dimethyl amine 0.00 74 0 N.D. 8) Phenol 0.00 94 0 N.D. 9) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 10) 2-Chlorophenol 0.00 128 0 N.D. 11) 1,3-Dichlorobenzene 0.00 146 0 N.D. 12) 1,4-Dichlorobenzene 0.00 146 0 N.D. 13) 1,2-Dichlorobenzene 0.00 146 0 N.D. 14) 2-Methylphenol 0.00 108 0 N.D. 15) 2,2’-oxybis(1-Chloropropan 0.00 45 0 N.D. 16) 3&4-Methylphenol 0.00 108 0 N.D. 17) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 18) Hexachloroethane 0.00 117 0 N.D. 21) Nitrobenzene 0.00 77 0 N.D. 22) Isophorone 0.00 82 0 N.D. (#) = qualifier out of range (m) = manual integration 22558.D NP101901.M Tue Oct 23 14:55:17 2001 Page 1
NYC-WTC_000067408
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NYC-WTC_000067408Source: NYC Law Department, mirrored locally
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NYC-WTC_000087659
Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 4, 2001.
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