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Pesticide reference standard analysis, sample AD22582, Sept 2001

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Reference standard testing results for pesticide analysis of sample AD22582, verifying analytical method performance with known compounds.

NYC-WTC_000063290–000063355

Folder label: “525 9/24/01 EX 9/29 - 9/30 Analysis

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Integration Report Quanfile: C8A0929 Quan Entries: 28 Comment: BOHLK; METHOD 525; INST 204; 09/29/01; C8 Sorted via: Entry Number t

No Name of Compound R Time Scan# Mode Peak Areja Pk Height

3 chrysene d-12(IS) 22:56 1376 Auto 2,648,262 1,124,278 4 p-terpheny1 d-14(IS) 21:01 1261 Auto 4,158,859 3,260,937 5 acenaphthene d-10(SURR 12:32 752 Auto 2,557,593 1,548,846 6 phenanthrene d-10(SURR 17:15 1035 Auto 3,877,059 1,713,235 7 chrysene d-12 (SURR) 22:56 1376 Auto 2,648,262 1,124,278 8 1,3-d imethy1-2-n itrobe 8:11 491 Auto 1,639,953 872,916 9 triphenyl phosphate (S 22:19 1339 Auto 1,886,613 664,682 10 perylene d-12 (SURR) 27:30 1650 Auto 1,476,526 287,704 11 hexachlorocyclopentad i 10:22 622 Auto 1,489,246 854,237 12 hexachlorobenzene 15:43 943 Auto 3,493,532 1,507,236 13 simazine 16:32 992 Auto 2,345,784 535,869 14 atrazine 16:42 1002 Auto 2,087,322 727,325 15 alachlor 18:37 1117 Auto 3,138,668 1,643,023 16 bis(2-ethyIhexy1)adipa 22:11 1331 Auto 5,958,378 2,448,333 17 bisC2-ethy1hexy1)phtha 23:14 1394 Auto 9,081,604 3,247,026 18 benzo(a)pyrene 27:16 1636 Auto 5,583,544 1,148,790 19 eptc 10:47 647 Auto 12,426,462 5,991,276 20 2,6-d ini troto1uene 12:09 729 Auto 2,767,870 1,774,324 21 2,4-d ini troto1uene 13:08 788 Auto 3,481,746 1,827,500 22 molinate 13:17 797 Auto 7,207,197 5,055,833 23 terbac i1 17:41 1061 Auto 1,945,792 549,167 c CD 24 acetochlor 18:26 1106 Auto 2,335,031 1,107,500 E 3 25 metribuzin 18:29 1109 Auto 4,261,205 2,541,176 o o 26 metolachlor 19:21 1161 Auto 9,077,493 5,290,441 Q 27 butachlor 20:33 1233 Auto 3,179,920 2,210,869 O) TO CO ■c o 28 4,4'-dde 20:57 1257 Auto 4,180,859 2,857,291 co co Q_ co o o o o 3 o CL o'

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