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Pesticide reference standard analysis, sample AD22582, Sept 2001

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Reference standard testing results for pesticide analysis of sample AD22582, verifying analytical method performance with known compounds.

NYC-WTC_000063290–000063355

Folder label: “525 9/24/01 EX 9/29 - 9/30 Analysis

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Integration Report Quanfile: C6A0929 Quan Entries: 28 Comment: BOHLK; METHOD 525; INST 204; 09/29/01; C6 Sorted uia: Entry Number t

No Name of Compound R T ime Scan# Mode Peak Areja PR Height

3 chrysene d-12CIS) 22:57 1377 Auto 2,745,751 1,285,774 4 p-terpheny1 d-14 CIS) 21:02 1262 Auto 3,895,571 2,846,568 5 acenaphthene d-10(SURR 12:33 753 Auto 2,657,450 1,271,428 6 phenanthrene d-10CSURR 17:16 1036 Auto 3,997,195 1,978,205 7 chrysene d-12 CSURR) 22:57 1377 Auto 2,745,751 1,285,774 8 1,3-d inethy1-2-n itrobe 8:12 492 Auto 1,631,671 934,285 9 triphenyl phosphate (S 22:19 1339 Auto 1,896,212 623,185 10 perylene d-12 CSURR) 27:31 1651 Auto 1,575,348 309,419 11 hexachlorocyclopentad i 10:23 623 Auto 554,056 386,652 12 hexachlorobenzene 15:43 943 Auto 1,393,903 591,208 13 simazine 16:30 990 Auto 951,592 272,241 14 atrazine 16:41 1001 Auto 830,299 333,072 15 alachlor 18:38 1118 Auto 1,347,447 923,913 16 b is (2-ethy Ihexy Dad ipa 22:11 1331 Auto 2,418,620 815,384 17 b is(2-ethyIhexy1)phtha 23:15 1395 Auto 3,882,977 1,131,895 18 benzo(a)pyrene 27:15 1635 Auto 2,283,482 438,203 19 eptc 10:47 647 Auto 5,208,375 3,104,052 20 2,6-d ini troto1uene 12:10 730 Auto 971,033 492,574 21 2,4-d ini troto1uene 13:09 789 Auto 1,350,795 845,833 22 molinate 13:18 798 Auto 2,543,926 1,488,405 23 terbaci1 17:39 1059 Auto 561,838 206,680 c o 24 acetochlor 18:27 1107 Auto 953,231 537,500 E 3 25 metribuzin 18:29 1109 Auto 1,748,26^ 1,106,333 o o 26 metolachlor 19:22 1162 Auto 3,861,24f; 1,768,461 Q 27 butachlor 20:34 1234 Auto 1,346,699 1,001,744 co co TO ■c o 28 4,4^-dde 20:57 1257 Auto 1,542,007 842,808 co co CL co o g o o Z 3 S' s 0.

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NYC-WTC_000063333Source: NYC Law Department, mirrored locally

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