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Pesticide reference standard analysis, sample AD22582, Sept 2001

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Reference standard testing results for pesticide analysis of sample AD22582, verifying analytical method performance with known compounds.

NYC-WTC_000063290–000063355

Folder label: “525 9/24/01 EX 9/29 - 9/30 Analysis

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Integration Report Quanfile: C2A0929 Quan Entries: 27 Comment: BOHLK; METHOD 525; INST 204; 09/29/01; C2 Sorted uia: Entry Number t

No Name of Compound R Time Scant! Node Peak Ar^a Pk Height

2 phenanthrene d-10 (IS) 17:16 1036 Auto 4,014,307 2,005,448 3 chrysene d-12(IS) 22:57 1377 Auto 2,651,387 1,265,406 4 p-terphenyl d-14(IS) 21:02 1262 Auto 3,513,399 2,165,725 5 acenaphthene d-10(SURR 12:33 753 Auto 2,679,696 1,263,782 6 phenanthrene d-10(SURR 17:16 1036 Auto 4,014,307 2,005,448 7 chrysene d-12 (SURR) 22:57 1377 Auto 2,651,387 1,265,406 8 1,3-d imethy1-2-n itrobe 8:12 492 Auto 1,701,656 990,000 9 triphenyl phosphate (S 22:20 1340 Auto 1,496,488 475,277 10 perylene d-12 (SURR) 27:31 1651 Auto 1,613,701 297,429 11 hexachlorocyclopentad i 10:23 623 Auto 5,128 3,826 12 hexachlorobenzene 15:43 943 Auto 28,951 11,756 13 simazine 16:29 989 Auto 12,046 3,675 14 atrazine 16:40 1000 Auto 11,106 4,248 15 alachlor 18:38 1118 Auto 23,609 12,117 16 bis(2-ethyIhexy1)adipa 22:11 1331 Auto 51,511 11,085 17 b is(2-ethyIhexy1)phtha 23:14 1394 Auto 85,016 14,540 18 benzo(a)pyrene 27:16 1636 Auto 45,260 5,673 19 eptc 10:47 647 Auto 246,766 113,699 20 2,6-d in itrotoluene 12:10 730 Auto 17,888 7,943 21 2,4-d in itrotoluene 13:09 789 Auto 17,654 6,360 22 molinate 13:17 797 Auto 50,547 22,854 c 23 acetochlor 18:27 1107 Auto 15,887 7,816 (D E 24 metribuzin 18:28 1108 Auto 22,883 9,755 3 o o 25 metolachlor 19:21 1161 Auto 66,8^ 25,654 Q 26 butachlor 20:34 1234 Auto 25,105 12,747 CM TO 27 4,4"-dde 20:57 1257 Auto 43,639 28,539 CO CO O CL CD o .2 o Z o 3 o CL oI 05 I6 o >- z z

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NYC-WTC_000063321Source: NYC Law Department, mirrored locally

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