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Method detection limit analysis, sample AD23260, October 2001

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Laboratory method detection limit (MDL) analysis for sample AD23260 establishing minimum quantifiable levels for multiple pesticides and herbicides, October 1-6, 2001.

NYC-WTC_000062278–000062287

Folder label: “525 10/1/01 EXT. 10/6/01 Analysis

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§ '2 o o Integration Report Quanfile: MDLB1006 Quan Entries: 28 ■D c CT o' o Connent: BOHLK; METHOD 525; INST 204; 10/06/01; MDL o> "0 ro o ro 00 Sorted via: Entry Nunber t 03 O No Name of Compound R Tine Scan# Mode Peak Area Pk Height o o c 3 o 3 chrysene d-12(IS) 22:58 1378 Auto 1,715,245 712,923 3 4 p-terphenyl d-14(IS) 21:02 1262 Auto 2,999,158 2,188,647 5 acenaphthene d-10(SURR 12:33 753 Auto 1,694,059 984,345 6 phenanthrene d-10(SURR 17:17 1037 Auto 2,488,351 1,101,219 7 chrysene d-12 (SURR) 22:58 1378 Auto 1,715,245 712,923 8 1,3-d inethy1-2-n itrobe 8:12 492 Auto 1,013,829 505,753 9 triphenyl phosphate CS 22:20 1340 Auto 1,324,356 517,825 10 perylene d-12 (SURR) 27:32 1652 Auto 1,426,750 262,209 11 hexachlorocyclopentad i 10:23 623 Auto 12,976 7,777 12 hexachlorobenzene 15:44 944 Auto 41,413 15,581 13 sinazine 16:31 991 Auto 26,726 6,238 14 atrazine 16:41 1001 Auto 15,872 4,921 15 alachlor 18:38 1118 Auto 37,196 20,712 16 bis(2-ethyIhexy1)adipa 22:12 1332 Auto 49,581 9,987 17 b is(2-ethyIhexy 1)phtha 23:15 1395 Auto 249,216 49,806 18 benzo(a)pyrene 27:18 1638 Auto 48,302 5,909 19 eptc 10:48 648 Auto 615,994 300,689 20 2,6-d ini troto1uene 12:10 730 Auto 212,885 104,364 21 2,4-d in itrotoluene 13:09 789 Auto 290,539 109,137 22 no1 inate 13:18 798 Auto 318,056 175,209 23 terbac i1 17:38 1058 Auto 170,042 50,163 24 acetochlor 18:27 1107 Auto 241,750 148,774 25 netribuzin 18:29 1109 Auto 28,813 13,652 26 netolachlor 19:22 1162 Auto 108,243 46,466 27 butachlor 20:34 1234 Auto 30,716 18,090 28 4,4"-dde 20:58 1258 Auto 151,150 86,171

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NYC-WTC_000062281Source: NYC Law Department, mirrored locally

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