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GCMS analysis results, sample AE06857, April 2002

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analytical results for sample AE06857 showing surrogate compound 2,4-DDD recovery at 90% with detection limit 10.0 ug, completed April 23, 2002

NYC-WTC_000060814–000060823

Folder label: “GCMS X 3/25/02 A 4/17/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\MSDCHEM\l\DATA\041702\6857.D Vial: 6 Acq Oh : 17 Apr 2002 12:43 pm Operator: Bohlk Sample .: sample 6857, FB 3/25/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 22 11:12:14 2002 Quant Results File: 5080402BBC.RES

Quant Method : C:\MSDCHEM\l\5973N\5080402BBC.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Tue Apr 16 18:27:45 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Compound R.T. Qlon Response Cone Unit Qvalue

46) Di-n-Octylphthalate 0.00 149 0 N.D. 47) Benzo (b) fluoranthene 0.00 252 0 N.D. 48) Benzo (k) fluoranthene 0.00 252 0 N.D. 49) Benzo (a) pyrene 0.00 252 0 N.D. d 50) Indeno (1,2,3-cd) pyrene 0.00 276 0 N.D. 51) Dibenz (a,h) anthracene 0.00 278 0 N.D. 52) Benzo (g,h,i) perylene 0.00 276 0 N.D.

{#) = qualifier out of range (m) = manual integration 6857.D 5080402BBC.M Mon Apr 22 11:13:34 2002 Page 2

NYC-WTC_000060818

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NYC-WTC_000060818Source: NYC Law Department, mirrored locally

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