GCMS Method 508 sample analysis results, April 9 2002

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LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\020409\6339.D Vial: 8 Acq On 9 Apr 2002 9:41 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\l\METHODS\SC7kNAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.314 21 40 49 PV 5 7623 315082 0.73% 0.148% 2 3.379 49 51 56 W 4 2188 42393 0.10% 0.020% 3 3.420 56 58 70 VB 4 2296 55831 0.13% 0.026% 4 5.036 327 333 337 PV 4 2052 41287 0.10% 0.019% 5 5.553 418 421 436 PV 2 28468 772211 1.78% 0.362%

6 5.653 436 438 445 W 3 3828 90998 0.21% 0.043% 7 5.700 445 446 453 W 4 2888 59525 0.14%. 0.028% 8 10.665 1277 1291 1314 PV 968370 27164466 62.62% 12.728% 9 15.776 2139 2161 2174 BV 1405406 35951159 82.87% 16.846% 10 16.000 2192 2199 2209 PV 2 1944 48913 0.11% 0.023%

11 23.673 3482 3505 3517 W 1510622 41980164 96.77% 19.670% 12 30.271 4619 4628 4636 BV 3 5832 149948 0.35% 0.070% 13 30.912 4717 4737 4765 PV 2 1349575 43381704 100.00% 20.327% 14 31.135 4765 4775 4786 W 9165 201621 0.46% 0.094% 15 36.623 5700 5709 5716 PV 135505 2161000 4.98% 1.013%

16 39.102 6121 6131 6157 PV 2 1875737 37259089 85.89% 17.458% 17 42.310 6659 6677 6704 PV 2 1205774 23732432 54.71% 11.120% 18 42.481 6704 6706 6708 W 2 1020 9128 0.02% 0.004%

Sum of corrected areas: 213416951

6339.D SCANAPR0902.M Thu May 02 14:06:59 2002 Page 1

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