GCMS Method 508 sample analysis results, April 9 2002

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LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\020409\6337.D Vial: 6 Acq On 9 Apr 2002 7:49 pm Operator: McLean Sample 3/18 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.e

Method : C:\MSDCHEM\1\METHODS\SCANAPR0902.M (Chemstation Integrator) Title : Method 508 GC/MS Scan

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 3.291 21 36 38 PV 3 6363 182794 0.43% 0.087% 2 3.320 38 41 45 W 2 11910 194185 0.46% 0.093% 3 3.355 45 47 . 49 W 2 3697 39933 0.09% 0.019% 4 3.373 49 50 53 W 2 3390 44686 0.10% 0.021% 5 3.426 56 59 72 W 5 3611 116948 0.27% 0.056%

6 3.520 72 75 81 W 3 2540 33615 0.08% 0.016% 7 5.547 410 420 448 PV 2 42152 1207901 2.83% 0.576% 8 5.729 448 451 460 W 4 2149 43828 0.10% 0.021% 9 10.664 1280 1291 1311 VV 998614 26569060 62.27% 12.667% 10 15.776 2145 2161 2185 W 1380174 35198855 82.49% 16.781%

11 15.988 2190 2197 2204 W 2 2314 62141 0.15% 0.030% 12 23.673 3487 3505 3522 PV 1467589 41318862 96.83% 19.699% 13 30.265 4616 4627 4640 PV 3 6217 165544 0.39% 0.079% 14 30.912 4718 4737 4750 W 2 1357751 42669692 100.00% 20.343% 15 31.135 4758 4775 4787 W 2 8005 210734 0.49% 0.100%

16 36.623 5703 5709 5722 W 152337 2505196 5.87% 1.194% 17 39.102 6120 6131 6161 PV 2 1836999 37197017 87.17% 17.734% 18 42.310 6662 6677 6702 PV 2 1097500 21985849 51.53% 10.482% 19 42.463 6702 6703 6706 W 2 1001 8310 0.02% 0.004%

Sum of corrected areas: 209755149

6337.D SCANAPR0902.M Thu May 02 14:04:56,2002 Page 1

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