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GCMS analysis results, sample AE06264, April 18, 2002

Machine-extracted title · confidence 80%

Gas chromatography-mass spectrometry analysis of sample AE06264 performed April 18, 2002, detecting unknown compounds and 2,4-DDD surrogate standard.

NYC-WTC_000060076–000060084

Folder label: “GCMS X 3/15/02 A 4/5/02

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Scanned page image, NYC-WTC_000060081
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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\040402B\6264.D Vial: 20 Acq On 5 Apr 2002. 11:04 am Operator: Bohlk Sample SAMPLE 6264 3/15/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080402.M {RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 . Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 9.460 1079 1086 1114 rBV 3024996 7678987 61.25% 12.352% 2 11.975 1506 1514 1524 rBV 284835 524557 4.18% 0.844% 3 12.938 1669 1678 1700 rBV 5460376 11408666 91.00% 18.351% 4 18.050 2537 2548 2573 rBV 6113864 12536424 100.00% 20.165% 5 22.410 3279 3290 3312 rBV2 5369064 12004234 95.75% 19.309%

6 27.357 4124 4132 4144 rBV 705986 1420478 11.33% 2.285% 7 30.236 4610 4622 4640 rBV2 4064835 9716899 77.51% 15.630% 8 34.114 5270 5282 5305 rBV2 2743093 6879783 54.88% 11.066%

Sum of corrected areas: 62170028

5264.D 5080402.M Fri Apr 05 17:16:49 2002 Page 1

NYC-WTC_000060081

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NYC-WTC_000060081Source: NYC Law Department, mirrored locally

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