GCMS analysis results, sample AE06264, April 18, 2002

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Gas chromatography-mass spectrometry analysis of sample AE06264 performed April 18, 2002, detecting unknown compounds and 2,4-DDD surrogate standard.

NYC-WTC_000060076–000060084

Folder label: “GCMS X 3/15/02 A 4/5/02”

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

.> Data File C:\MSDCHEM\l\DATA\040402B\6264.D vial: 20 Acq On 5 Apr 2002 11:04 am Operator: Bohlk Sample SAMPLE 6264 3/15/02 'Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: BENZO.P Quant Time: Apr 05 17:14:53 2002 Quant Results File: 5080402.RES

Quant Method : C:\MSDCHEM\i\5973N\5080402.M (RTE Integrator) Title : Quantitation For Method 508gcscan Last Update : Fri Apr 05 05:56:22 2002 Response via : Initial Calibration DataAcq Meth : 508SCAN

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 9.46 152 1138048 20.00 ug/L -0.01 10) Naphthalene-d8 12.94 136 5196296 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.05 164 2880005 20.00 ug/L 0.00 29) Phenanthrene-dl0 22.41 188 4056268 20.00 ug/L -0.01 38) Chrysene-dl2 30.23 240 3012792 20.00 ug/L -0.02 44) Perylene-dl2 34.11 264 1775251 20.00 ug/L 0.00

System Monitoring Compounds 37) 2,4-DDD (StJRR) 27.36 235 241135 5.99 ug/L 0.00 Spiked Amount 5.000 Recovery = 119.80%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 ' - oxybis (1-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene o.ob 162 0 N.D. 20) Dimethylphthalate 0.00 .163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 2 8). Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 24.58 149 4520 0.03 ug/L 79 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 . N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 0.00 149 0 N.D. 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.

(#) = qualifier out of range (m) = manual integration 6264.D 5080402.M Fri Apr 05 17:16:43 2002 Page 1

NYC-WTC_000060078

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GCMS analysis results for sample AE06265, April 2002 · Box DEP Box 57

NYC-WTC_000060085

Laboratory report documenting GCMS analysis of environmental sample AE06265 conducted on April 18, 2002.

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