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GCMS analysis results, sample AE05918, April 2002

Machine-extracted title · confidence 87%

Gas chromatography-mass spectrometry analysis of sample AE05918 showing detection of unknown compounds and 2,4-DDD surrogate, completed April 5, 2002.

NYC-WTC_000059853–000059867

Folder label: “GCMS X 3/14/02 A 3/23/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File : C:\MSDCHEM\l\DATA\032202\5918.D Vial: 12 Acq On : 23 Mar 2002 4:21 am Operator: McLean Sample : SAMPLE 5918 3/14/02 Inst : Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

■If leading or trailing edge < 100 prefer < Baseline drop else tangent Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 ' 5.664 437 440 453 rBV 49568 129415 1.25% 0.256% 2 9.548 1094 1101 1127 rBV 2506499 6453963 62.58% 12.775% 3 13.026 1684 1693 1703 rBV 4654673 9275285 89.94% 18.360% 4 13.097 1703 1705 1716 rVB4 157539 348516 3.38% 0.690% 5 18.138 2553 2563 2586 rBV 5023741 10312754 100.00% 20.413%

6 22.498 3295 3305 3325 rBV2 4520913 10191554 98.82% 20.173% 7 24.161 3583 3588 3596 rBV3 77320 152496 1.48% 0.302% 8 27.433 4137 4145 4157 rBV2 532237 1098568 10.65% 2.175% 9 30.312 4623 4635 4653 rBV2 3441158 7980160 77.38% 15.796% 10 34.184 5283 5294 5313 rBV2 1855531 4577491 ■44.39% 9.061%

Sum of corrected areas: 50520202

5918.D 5080302.M Fri Apr 05 07:33:29 2002 Page 1

NYC-WTC_000059863

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NYC-WTC_000059863Source: NYC Law Department, mirrored locally

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