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GCMS analysis results for sample AE01156, March 29 2002

Machine-extracted title · confidence 100%

Gas chromatography-mass spectrometry analysis of sample AE01156 conducted March 29, 2002, showing surrogate standard 2,4-DDD recovery.

NYC-WTC_000059693–000059702

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2102\1156.D Vial: 19 Acq On : 22 Mar 2002 5:02 am Operator: Sample : re-extract Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 259:092002 <Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.73 178 937 N.D. 34) Anthracene 25.85 178 538 N.D. 35) Di-n-butylphthalate 27.63 149 4493 N.D. 36) Fluoranthene 29.36 202 327 N.D. 39) Pyrene 30.02 202 598 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.72 228 4360 N.D. 42) Bis(2-ethylhexyl)phthalate 33.93 149 8975 N.D. 43) Chrysene 33.79 228 1190 N.D. 45) Di-n-Octylphthalate 35.67 149 339 N.D. 46) Benzo(b)fluoranthene 36.78 252 883 N.D. 47) Benzo(k)fluoranthene 36.84 252 808 N.D. 48) Benzo(a)pyrene 37.79 252 519 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 '0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 1156.D GCMS0308.M Mon Mar 25 09:13:23 2002 Page 2

NYC-WTC_000059696

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NYC-WTC_000059696Source: NYC Law Department, mirrored locally

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