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GCMS reference data for sample AE01156, March 25 2002

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Reference data report listing component names and response values for calibration verification conducted on March 25, 2002.

NYC-WTC_000059679–000059686

Folder label: “GCMS X 3/13/02 A 3/27/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\iyiAR2502\REF2.D Vial: 8 Acq On : 25 Mar 2002 12:09 pm Operator: Sample : re-inject Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 25 13:59 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title , : 209 625/TCLP calibration table Last Update : Fri Mar 08 08:54:27 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 23.22 168 150553 7.65 ug/1 # 81 31) 4-Bromophenyl-phenylether 24.30 248 103637 8.96 ug/1 # 86 32) Hexachlorobenzene 24.73 284 125035 9.31 ug/1 # 87 3 3) Phenanthrene 25.70 178 550323 8.74 ug/1 98 34) Anthracene 25.83 178 500476 8.02 ug/1 100 35) Di-n-butylphthalate 27.60 149 700161 8.84 ug/1 # 97 36) Fluoranthene 29.33 202 550152 8.33 ug/1 95 3 9) Pyrene 30.01 202 559116 11.29 ug/1 96 40) Butylbenzylphthalate 32.14 149 261075 10.22 ug/1 95 41) Benzo(a)anthracene 33.65 228 347229 8.43 ug/1 99 42) Bis(2-ethylhexyl)phthalate 33.91 149 361027 10.47 ug/1 99 43) Chrysene 33.77 228 360366 8.92 ug/1 99 45) Di-n-Octylphthalate 35.66 149 • 435485 9.63 ug/1 # 97 46)- Benzo(b)fluoranthene 36.76 252 275929 8.80 ug/1 98 47) Benzo(k)fluoranthene 36.82 252 276255 9.04 ug/1 97 48) Benzo(a)pyrene 37.75 252 191071 6.69 ug/1 # 97 49) Indeno(1,2,3-cd)pyrene 42.06 276 187-751 5.44 ug/1 97 50) Dibenz(a,h)anthracene 42.14 278 156154 5.85 ug/1 99 51) Benzo(g,h,i)perylene 43.30 276 174063 6.19 ug/1 94

(#) = qualifier out of range (m) = manual integration REF2.D GCMS0308.M Mon Mar 25 14:00:18 2002 Page 2

NYC-WTC_000059682

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NYC-WTC_000059682Source: NYC Law Department, mirrored locally

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