NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\MSDCHEM\1\DATA\O317oA5512.D Vial: 13
Acq On 17 Mar 2002 6:35 pm Operator: McLean
Sample 3/11/02 Inst Instrumen
Mise Multiplr: 1.00
MS Integration Params: BENZO.P
I
Quant Time: Mar 25 06:52:31 2002 Quant Results File: 5080302.RES
Quant Method C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator)
Title Quantitation For Mettiod 508gcscan
Last Update Thu. Mar 14 13:02:27 2002
Response via Initial Calibration
DataAcq Meth 508SCAN I
I
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 150 1657916 20.00 ug/L 0.00
10) Naphthalene-d8 13.03 136 4481940 20.00 ug/L 0.00
17) Acenaphthene-dlO 18.13 164 2498294 20.00 ug/L 0.00
29) Phenanthrene-dlO 22.50 188 3804572 20.00 ug/L 0.00
38) Chrysene-dl2 30.30 240 3536156 20.00 ug/L -0.02
44) Perylene-dl2 34.18 264 1948014 20.00 ug/L 0.00
System Monitoring Compounds
37) 2,4-ddd surr
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27^.43 235 347936 7.67 ug/L 0.00
Spiked Amount 5.000 Recovery = 153.40%
Target Compounds I ■ Qvalue
2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d
3) bis(2-chloroethyl) ether 6.00 93 0 N.D.
4) 1,3 - Dichlorobenze 0.00 146 0 N.D.
5) 1,4 - Dichlorobenzene 0.00 146 0 N.D.
6) 1,2 - Dichlorobenzene 0.00 146 0 N.D.
7) 2,2 ' - oxybis (1-Chloropr 6.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 6.00 117 0 N.D.
11) Nitrobenzene 6.00 77 0 N.D.
12) Isophorone 6.00 82 0 N.D.
13) bis(2-Chloroethoxy) methan ■ 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 6.00 128 0 N.D.
16) Hexachlorobutadiene 6.0 0 225 0 N.D.
18) Hexachlorocyclopentadiene 6.00 237 0 N.D.
19) 2-chloronaphthalene 0,. 00 162 0 N.D.
20) Dimethylphthalate o'. 00 163 0 N.D.
21) 2,6-Dinitrotoluene o'. 00 165 0 N.D. d
22) Acenaphthylene 6.00 152 0 N.D.
23) Acenaphthene 6.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 0,. 00 149 0 N.D.
26) 4-Chlorophenyl-phenyl ethe 6.00 204 0 N.D.
27) Fluorene o'. 00 166 0 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
30) N-Nitrosodiphenylamine 0.00 169 0 N.D.
31) 4-Bromophenyl-phenyl ether 0.0 0 248 0 N.D.
32) Hexachlorobenzene o'. 00 284 0 N.D.
33) Phenanthrene 6.00 178 0 N.D.
34) Anthracene o'. 00 178 0 N.D.
35) Di-n-butylphthalate 24'. 64 149 115302 0.57 ug/L 98
36) Fluoranthene o'. 00 202 0 N.D.
39) Pyrene O'. 00 . 202 0 N.D.
40) Butylbenzylphthalate o'. 00 149 0 N.D.
41) Benzo (a) antracene o'. 0 0 228 0 N.D. d
42) Bis (2-ethylhexyl) phthala 30'. 92 149 20273 0.15 ug/L 90
43) Chrysene o'. 00 228 0 N.D. d
45) Di-n-Octylphthalate o'. 00 149 0 N.D.
46) Benzo (b) fluoranthene 0.00 252 0 N.D.
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(#) = qualifier out of range (m) = manual integration
5512.D 5080302.M Mon Mar 25 06:53:11 2002 Page 1
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■ NYC-WTC_000059422
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