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GCMS unknown compound analysis, sample AE05304, March 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry analysis of sample AE05304 conducted on 3/29/2002, testing for unknown organic compounds.

NYC-WTC_000059369–000059378

Folder label: “GCMS X 3/11/02 A 3/17/02

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NYC 9/11 Public Portal Document

LSC Area Percent Report

Data File C:\MSDCHEM\l\DATA\031702\5304.D Vial: 7 Acg On 17 Mar 2002 1:42 pm Operator: McLean Sample 3/11/02 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method C:\MSDCHEM\1\5973N\568O3O2.M (RTE Integrator) Title Quantitation For Method 508gcscan Smoothing OFF Filtering: 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs 0.2 Max Peaks: 100 Stop Thrs 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.561 271 274 279 rBV 185628 410443 4.29% 0.803% 2 9.543 708 713 736 rBV 2333688 6304807 65.86% 12.329% 3 12.056 985 990 999 rBV 220745 407519 4.26% 0.797% 4 13.026 1091 1097 1111 rBV 4260762 8656201 90.43% 16.927% 5 18.133 1654 1660 1678 rBV 4606224 9436215 98.57% 18.453%

6 22.495 2134 2141 2155 rBV2 4435594 9572741 100.00% 18.720% 7 22.650 2155 2158 2169 rVB3 38363 124530 1.30% 0.244% 8 27.430 2680 2685 2693 rBV 837003 1631827 17.05% 3.191% 9 30.305 2995 3002 3024 rBV2 3912496 9177779 95.87% 17.947% 10 34.178 3422 3429 3452 rBV 2263954 5414854 56.57% 10.589%

Sum of corrected areas: 51136916

5304.D 5080302.M Fri Mar 22 10:14:53 2002 Page 1

NYC-WTC_000059374

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NYC-WTC_000059374Source: NYC Law Department, mirrored locally

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