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GCMS unknown compound analysis, sample AE05516, April 2002

Machine-extracted title · confidence 100%

Laboratory record of gas chromatography mass spectrometry analysis for unknown compounds and surrogates on April 9, 2002.

NYC-WTC_000059286–000059295

Folder label: “GCMS X 3/11/02 A 4/1/02

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Scanned page image, NYC-WTC_000059291
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report 4 Data File C:\HPCHEM\1\DATA\APRO102\5516.D Vial: 7 Acq On 1 Apr 2002 6:11 pm • Operator: Sample gc/ms scan 3/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0403.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.133 331 336 349 rBV 201671 512289 11.37% 2.453% 2 8.280 349 352 363 rVB2 26640 70691 1.57% 0.339% 3 12.246 779 784 800 rVB 1278700 3069211 68.12% 14.698% 4 15.881 1174 1180 1197 rBV 1835682 3981112 88.36% 19.065% 5 21.197 1752 1759 1771 rBV 2097596. 4505338 100.00% 21.575%

6 25.640 2236 2243 2254 rBV 1963973 4226219 93.80% 20.239% 7 30.707 2790 2795 2801 rBV 221612 443074 9.83% 2.122% 8 33.691 3113 3120 3139 rBV2 1054364 2467037 54.76% 11.814% 9 37.942 3574 3583 3604 rBV2 536567 1606985 35.67% 7.696%

Sum of corrected areas: 20881956

5516.D GCMS0403.M Thu Apr 04 13:54:01 2002

NYC-WTC_OO6O5929T

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NYC-WTC_000059291Source: NYC Law Department, mirrored locally

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