GCMS analysis results, sample AE05242, March 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

■ Data' File : C:\MSDCHEM\l\DATA\031602\5242.D Vial: 19 Acq On : 17 Mar 2002 1:35 am Operator: McLean Sample : 3/9 Inst Instrumen Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title : Quantitation For Method 508gcscan ' • Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak corr. corr. % of # min scan scan scan TY height area % max. total

1 5.570 272 275 294 rBV 134144 383219 3.73% 0.702% 2 9.543 709 713 730 rBV 2520597 6648508 64.67% 12.187% 3 13.026 1091 1097 1111 rBV 4569292 9356644 91.01% 17.151% 4 18.133 1654 1660 1677 rBV 4909142 10067698 97.92% 18.454% 5 22.495 2135 2141 2155 rBV2 4681454 10281233 100.00% 18.846%

6 22.650 2155 2158 2168 rVB 40148 115747 1.13% 0.212% 7 27.430 2680 2685 2701 rVB 648564 1260169 12.26% 2.310% 8 30.305 2995 3002 3027 rBV2 4154974 9989617 97.16% 18.311% 9 34.178 3421 3429 3459 rBV2 2493021 6451790 62.75% 11.826%

Sum of corrected areas: 54554625

V

5242.D 5080302.M Wed Mar 20 08:52:20 2002 Page 1

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