Laboratory report showing non-detect levels for various organic compounds in a GCMS blank sample from March 2002.
NYC-WTC_000059028–000059035Folder label: “GCMS X 3/9/02 A 3/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File C:\MSDCHEM\1\DATA\031602\0309LB.D Vial: 14 Acq On 16 Mar 2002 9:31 pm Operator: McLean Sample 3/9 Inst : Instrumen Mise Multiplr: 1.00 , MS Integration Params: BENZO.P Quant Time: Mar 20 08:20:29 2002 Quant Results File; 5080302.RES
Quant Method C:\MSDCHEM\l\5973N\5080302.M (RTE Integrator) Title Quantitation For Method 508gcscan Last Update Thu Mar 14 13:02:27 2002 Response via Initial Calibration DataAcq Meth 508SCAN
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 9.54 150 1352835 20.00 ug/L 0.00 10) Naphthalene-d8 13.03 136 3779883 20.00 ug/L 0.00 17) Acenaphthene-dlO 18.13 164 2085523 20.00 ug/L 0.00 29) Phenanthrene-dlO 22.50 188 3203603 20.00 ug/L 0.00 38) Chrysene-dl2 30.30 240 2918232 20.00 ug/L -0.02 44) Perylene-dl2 34.18 264 1533621 20.00 ug/L 0.00
System Monitoring Compounds 37) 2,4-ddd surr 27.43 235 266306 6.97 ug/L 0.00 Spiked Amount 5.000 Recovery = 139.40%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. d 3) bis(2-chloroethyl) ether 0.00 93 0 N.D. 4) 1,3 - Dichlorobenze 0.00 146 0 N.D. 5) 1,4 - Dichlorobenzene 0.00 146 0 N.D. 6) 1,2 - Dichlorobenzene 0.00 146 0 N.D. 7) 2,2 ' - oxybis (1-Chloropr 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy) methan 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 0.00 128 0 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. d 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 0.00 149 0 N.D. 26) 4-Chlorophenyl-phenyl ethe 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. 30) N-Nitrosodiphenylamine 0.00 169 0 N.D. 31) 4-Bromophenyl-phenyl ether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 0.00 178 0 N.D. 35) Di-n-butylphthalate 0.00 149 0 N.D. d 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo (a) antracene 0.00 228 0 N.D. d 42) Bis (2-ethylhexyl) phthala 0.00 149 0 N.D. 43) Chrysene 0.00 228 0 N.D. d 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo (b) fluoranthene 0.00 252 0 N.D.
(#) = qualifier out of range (m) = manual integration 0309LB.D 5080302.M Wed Mar 20 08:21:35 2002 Page 1
NYC-WTC_000059029
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NYC-WTC_000059048
GCMS analysis of sample AE05238 performed on 3/29/02 showing 2,4-DDD surrogate compound recovery at 152% with unspecified qualifier flag.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059338
Laboratory report showing blank sample analysis for volatile organic compounds using GCMS on March 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059075
Laboratory report documenting GCMS analysis of sample AE05241 for unknown compounds and surrogates on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059066
Laboratory report documenting GCMS analysis of sample AE05240 for unknown compounds and surrogates on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059093
Laboratory report documenting GCMS analysis of sample AE05301 for unknown compounds on March 29, 2002.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059440
Laboratory report documenting GCMS analysis of sample AE05514 conducted on March 29, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000059410
Laboratory report documenting GCMS analysis of sample AE05309 conducted on March 29, 2002, identifying unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.992
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039222
Laboratory report for sample AE06267 blank showing non-detect levels for volatile organic compounds analyzed on March 20, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000039109
GCMS blank analysis report for sample AE05902 showing results below detection limits for multiple volatile organic compounds on March 20, 2002.
1 shared topics · similarity 0.994
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000052435
Quality control blank report for GCMS analysis of sample AE01641 showing no detected compounds above the method detection limit.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000011960
Laboratory data sheet recording drip rates and pH values for samples analyzed by the DEP Labs between February and March 2002.
1 shared topics · similarity 0.993
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000037567
Laboratory report documenting GCMS analysis of sample AE03737 for unknown compounds and surrogates conducted on March 29, 2002.
1 shared topics · similarity 0.993
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Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in March 2002.
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Calibration results for specific volatile organic compounds used to verify GCMS instrument performance in March 2002.
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NYC-WTC_000059048
GCMS analysis of sample AE05238 performed on 3/29/02 showing 2,4-DDD surrogate compound recovery at 152% with unspecified qualifier flag.
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