GCMS analysis page for sample AE05051, April 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR3002\5051.D Vial: 24 Acq On : 30 Mar 2002 1:47 pm Operator: Sample : gc/ms scan 3/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 30 14:36 2002 Quant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)'

1) 1,4-Dichlorobenzene-d4 12.25 152 479884 20.00 ug/1 -0.10 10) Naphthalene-d8 15.89 136 1756834 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.19 164 990008 20.00 ug/1 -0.12 29) Phenanthrene-dlO 25.63 188 1367859 20.00 ug/1 -0.13 38) Chrysene-dl2 33.70 !24O 665402 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 1264 365989 20.00 ug/1 -0.19

System Monitoring Compounds 37) 2,4-DDD 30.71 •235 76355 5.56 ug/mL 0.21 Spiked Amount 5.000 . Recovery = 111.20%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 0.00 74 0 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichl'orobenzene 12.30 146 410 N.D. 5) 1,4-Dichlorobenzene 12.30 146 410 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 145 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 I 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.. 00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene . 0.00 ;.80 0 N.D. 15) Naphthalene 15.95 128 312 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 ]]62 0 N.D. .20) Dimethylphthalate 0.00 ]J63 0 N.D. 21) 2,6-Dinitrotoluene 0.00 3!65 0 N.D. 22) Acenaphthylene 0.00 1152 0 N.D. 23) Acenaphthene 0.00 1I53 0 N.D. 24) 2,4-Dinitrotoluene 0.00 ll65 0 N.D. 25) Diethylphthalate 22.67 1I49 477 N.D. 26) 4-Chlorophenyl-phenylether 0.00 2’04 0 N.D. 27) Fluorene 0.00 1*66 0 N.D. I 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D. _|__. (#) = qualifier out of range (m) = manual integration 5051.D GCMS0308.M Tue Apr 02 14:05:13 2002 Page 1

NYC-WTC_000058881