GCMS analysis page, sample AE04848, March 2002

NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2602\4848.D Vial: 21 Acq On : 27 Mar 2002 5:32 am Operator: Sample : gc/ms scan 3/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 29 11:21 2002 iQuant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.25 152 682842 20.00 ug/1 -0.10 10) Naphthalene-d8 15.88 136 2603147 20.00 ug/1 -0.11 17) Acenaphthene-dlO 21.20 164 1398543 20.00 ug/1 -0.11 29) Phenanthrene-dlO 25.64 188 2029871 20.00 ug/1 -0.12 38) Chrysene-dl 2 33.69 240 1046605 20.00 ug/1 -0.15 44) Perylene-dl2 37.94 264 578371 20.00 ug/1 -0.18

System Monitoring Compounds 37) 2,4-DDD 30.71 235 86533 4.25 ug/mL 0.21 Spiked Amount 5.000 Recovery = 85.00%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.49 74 201 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 ■ N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone. 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. .14) 1,2,4-Trichlorobenzene d. 00 180 0 N.D. 15) Naphthalene 15.95 128 454 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 . 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 21.52 165 285 N.D. 25) Diethylphthalate 22.68 149 470 n.d; 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 4848.D GCMS0308.M Fri Mar 29 11:22:50 2002 Page 1

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