GCMS analysis results for sample AE04943, April 2002

NYC 9/11 Public Portal Document

LSC Area Percent Report

* Data File : C:\HPCHEM\l\DATA\MAR3002\4943.D Vial: 10 Acq On : 29 Mar 2002 11:53 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSGINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering: 5 Sampling : 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 12.245 779 784 801 rVB 1130139 2726023 68.70% 14.983% 2 14.843 1062 1067 1073 rBV 156955 312314 7.87% 1.717% 3 15.889 1174 1181 1193 rBV 1611650 3472769 87.52% 19.087% ■ 4 21.195 1752 1759 1778 rBV 1844336 3967948 100.00% 21.809% 5 25.639 2236 2243 2252 rBV2 1669926 3685121 92.87% 20.254%

6 30.706 2790 2795 2803 rBV 226818 438929 11.06% 2.412% 7 33.690 3113 3120 3131 rBV2 931188 2076574 52.33% 11.413% 8 36.178 3385 3391 3402 rBV 52346 138734 . 3.50% 0.763% 9 37.931 3575 3582 3600 rBV2 462777 1375713 34.67% 7.561%

Sum of corrected areas: 18194125

4943.D GCMS0308.M Tue Apr 02 11:06:42 2002

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