NYC-WTC_000058687
GCMS analysis report for sample AE04946 conducted on April 5, 2002.
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GCMS sample analysis summary, April 2002
Machine-extracted title · confidence 100%Summary page for GCMS analysis of sample AE04941 conducted on April 5, 2002.
NYC-WTC_000058649–000058658Folder label: “GCMS X 3/6/02 A 3/30/02”
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NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR3002\4941.D Vial: 8 Acq On : 29 Mar 2002 9:53 pm Operator: Sample : gc/ms scan 3/6 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 2 10:46 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308
Internal Standards ■R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 460806 20.00 ug/1 -0.11 10) Naphthalene-d8 15.88 136 1686313 20.00 ug/1 -0.12 17) Acenaphthene-dlO 21.19 164 945953 20.00 ug/1 -0.13 29) Phenanthrene-dlO 25.63- 188 1331696 20.00 ug/1 -0.13 38) Chrysene-dl2 33.69 240 673352 20.00 ug/1 -0.15 44) Perylene-dl2 37.93 264 367518 20.00 ug/1 -0.19
System Monitoring Compounds 37) 2,4-DDD 30.71 235 78650 5.89 ug/mL 0.21 Spiked Amount 5.000 Recovery = 117.80%
Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.50 74 293 N.D. 3) bis(2-Chloroethyl)ether 0.00 93 0 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) Isophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 15.95 128 585- N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 0.00 163 0 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 22) Acenaphthylene 0.00 152 0 N.D. 23) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.68 149 572 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 0.00 166 0 N.D. 28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration 4941.D GCMS0308.M Tue Apr 02 10:47:17 2002 Page 1
NYC-WTC_000058651
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