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GCMS chromatogram data for sample AE04590, April 2002

Machine-extracted title · confidence 100%

Analytical run record from April 2, 2002, documenting unknown compounds and surrogate recovery for sample AE04590.

NYC-WTC_000058372–000058381

Folder label: “GCMS X 3/4/02 A 3/26/02

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Scanned page image, NYC-WTC_000058377
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

LSC Area Percent Report

• Data File ; C:\HPCHEM\l\DATA\MAR2602\4590.D Vial: 6 Acq On : 26 Mar 2002 2:39 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Smoothing : OFF Filtering : 5 Sampling 1 Min Area: 1 % of largest Peak Start Thrs: 0.2 Max Peaks: 100 Stop Thrs : 0 Peak Location: TOP

If leading or trailing edge < 100 prefer < Baseline drop else tangent > Peak separation: 5

Signal : TIC

peak R.T. first max last PK peak peak peak % of # min scan scan scan TY height area % max. total

1 8.136 332 337 349 rBV 113012 271111 5.96% 1.278% 2 8.283 349 353 366 rVB2 19493 54670 1.20% 0.258% 3 12.249 780 785 801 rVB 1331503 3110886 68.40% 14.662% 4 15.884 1175 1181 1199 rBV 1999548 4172825 91.75% 19.667% 5 21.190 1753 1759 1772 rBV 2104927 4547881 100.00% 21.434%

6 25.634 2236 2243 2253 rBV2 1964123 4270368 93.90% 20.126% 7 30.710 2791 2796 2805 rBV 251798 499268 10.98% 2.353% 8 33.694 3112 3121 3135 rBV2 1144798 2574130 56.60% 12.132% 9 37.935 3575 3583 3605 rBV2 568151 1716554 37.74% 8.090%

Sum of corrected areas: 21217693

4590.D GCMS0308.M Thu Mar 28 16:25:04 2002

NYC-WTC_000058377

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NYC-WTC_000058377Source: NYC Law Department, mirrored locally

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