NYC 9/11 Public Portal Document
Quantitation Report (QT Reviewed)
Data File : C:\HPCHEM\l\DATA\MAR2602\4590.D Vial: 6
Acq On : 26 Mar 2002 2:39 pm Operator:
Sample : gc/ms scan 3/4 Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: GOOFY.P
Quant Time: Mar 26 15:28 2002 Quant Results File: GCMS0308.RES
Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator)
Title : 209 625/TCLP calibration table
Last Update :■ Tue Mar 26 14:13:06 2002
Response via : Initial Calibration
DataAcq Meth : GCMS0308
Internal Standards R.T. Qlon Response Cone Units Dev(Min)
1) 1,4-Dichlorobenzene-d4 12.25 152 576964 20.00 ug/1 -0.10
10) Naphthalene-d8 15.88 136 2204855 20.00 ug/1 -0.11
17) Acenaphthene-dlO 21.19 164 1184035 20.00 ug/1 -0.12
29) Phenanthrene-dlO 25.63 188 1700728 20.00 ug/1 -0.13
38) Chrysene-dl2 33.69 240 889980 20.00 ug/1 -0.15
44) Perylene-dl2 37.94 264 502638 20.00 ug/1 -0.19
System Monitoring Compounds 1
37) 2,4-DDD 30.71 235 100757 ug/mL . ___
0.21
Spiked Amount 5.000 Recovery
Target Compounds Qvalue
2) N-nitroso-dimethyl amine 5.49 74 319 N.D.
3) bis(2-Chloroethyl)ether 0.00 93 0 N.D.
4) 1,3-Dichlorobenzene 0.00 146 0 N.D.
5) 1,4-Dichlorobenzene 0.00 146 0 N.D.
6) 1,2-Dichlorobenzene 0.00 146 0 N.D.
7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D.
8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D.
9) Hexachloroethane 0.00 117 0 N.D.
11) Nitrobenzene 0.00 77 0 N.D.
12) Isophorone 14.60 82 388 N.D.
13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D.
14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D.
15) Naphthalene 15.95 128 620 N.D.
16) Hexachlorobutadiene 0.00 225 0 N.D.
18) Hexachlorocyclopentadiene 0.00 237 0 N.D.
19) 2-Chloronaphthalene 0.00 162 0 N.D.
20) Dimethylphthalate 20.54 163 944 N.D.
21) 2,6-Dinitrotoluene 0.00 165 0 N.D.
22) Acenaphthylene 0.00 152 0 N.D.
23) Acenaphthene 0.00 153 0 N.D.
24) 2,4-Dinitrotoluene 0.00 165 0 N.D.
25) Diethylphthalate 22.67 149 1426 N.D.
26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D.
27) Fluorene 22.82 166 340 N.D.
28) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.
(#) = qualifier out of range (m) = manual integration
4590.D GCMS0308.M Thu Mar 28 15:38:22 2002 Page 1
NYC-WTC_000058374
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