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GCMS analysis results, sample AE04734, Apr 2002

Machine-extracted title · confidence 90%

Gas chromatography-mass spectrometry analysis of environmental sample AE04734 conducted April 4, 2002, detecting unknown compounds and surrogates.

NYC-WTC_000058274–000058282

Folder label: “GCMS X 3/4/02 A 3/23/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File : C:\HPCHEM\l\DATA\MAR2802\4734.D Vial: 7 Acq On : 28 Mar 2002 2:28 pm Operator: Sample : gc/ms scan 3/4 Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: GOOFY.P Quant Time: Apr 1 9:52 2002 iQuant Results File: GCMS0308.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update ; Fri Mar 29 10:31:28 2002 Response via : Initial Calibration DataAcq Meth : GCMS0308

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 0.00 178 0 N.D. 34) Anthracene 25.64 178 113 N.D. 35) Di-n-butylphthalate 27.61 149 1972 N.D. 36) Fluoranthene 0.00 202 0 N.D. 39) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 32.12 149 193 N.D. 41) Benzo(a)anthracene 33.69 228 2064 N.D. 42) Bis(2-ethylhexyl)phthalate 33.91 149 1616 N.D. 43) Chrysene 33.77 228 1149 N.D. 45) Di-n-Octylphthalate 35.66 149 176 N.D. 46) Benzo(b)fluoranthene 36.76 252 653 N.D. 47) Benzo(k)fluoranthene 36.76 252 1296 N.D. 4 8) Benzo(a)pyrene 37.75 252 198 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 4734.D GCMS0308.M Mon Apr 01 09:53:12 2002 Page 2

NYC-WTC_000058277

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NYC-WTC_000058277Source: NYC Law Department, mirrored locally

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